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Determination of acid volatile sulphur in river sediments by ICP-OES coupled with purge and trap method

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F62243136%3A_____%2F15%3AMSM08CL" target="_blank" >RIV/62243136:_____/15:MSM08CL - isvavai.cz</a>

  • Result on the web

    <a href="http://www.tandfonline.com/doi/abs/10.1080/03067319.2015.1085522" target="_blank" >http://www.tandfonline.com/doi/abs/10.1080/03067319.2015.1085522</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1080/03067319.2015.1085522" target="_blank" >10.1080/03067319.2015.1085522</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Determination of acid volatile sulphur in river sediments by ICP-OES coupled with purge and trap method

  • Original language description

    The developed and tested method is based on the acid volatile sulphur (AVS) releasing from a sample of sediment by acidification with hydrochloric acid and sequential absorption of released hydrogen sulphide into the absorption solution of sodium hydroxide. Total sulphur absorbed in the absorption solution is subsequently determined by inductively coupled plasma optical emission spectrometry (ICP-OES) technique. The method was tested using both model and real samples of the river sediment. Obtained results were compared with the results of iodometric determination as the method routinely used for the AVS determination. In case of using ICP-OES with purge and trap, there is no spectral interference of calcium; therefore for the determination of sulphur,it is possible to use atomic emission line of sulphur S I 180.7 nm. The tested method provides the results comparable with the iodometric method within the range of tested concentrations.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CB - Analytical chemistry, separation

  • OECD FORD branch

Result continuities

  • Project

    <a href="/en/project/ED2.1.00%2F03.0071" target="_blank" >ED2.1.00/03.0071: Unipetrol Centre of Research and Education</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2015

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    International Journal of Environmental Analytical Chemistry

  • ISSN

    0306-7319

  • e-ISSN

  • Volume of the periodical

    95

  • Issue of the periodical within the volume

    12

  • Country of publishing house

    GB - UNITED KINGDOM

  • Number of pages

    9

  • Pages from-to

    1090-1098

  • UT code for WoS article

  • EID of the result in the Scopus database