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Diphosphinoazine Rhodium(I) and Iridium(I) Complexes

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F67985858%3A_____%2F06%3A00049450" target="_blank" >RIV/67985858:_____/06:00049450 - isvavai.cz</a>

  • Alternative codes found

    RIV/00216208:11310/06:10720

  • Result on the web

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    Diphosphinoazine Rhodium(I) and Iridium(I) Complexes

  • Original language description

    The first rhodium complexes of diphosphinoazines [{RhCl(1,2-h:5,6-h- CH=CHCH2CH2CH=CHCH2CH2 )}2{m-R2PCH2C(But)=NN=C(But)CH2PR2] (R = Ph, Cy, Pri) were prepared by cleavage of the bridge in chloro(cycloocta-1,5-diene)rhodium(I) dimer, the analogous iridium(I) complexes were also prepared for the first time. The X-ray structures of isostructural rhodium and iridium complexes with bis(dicyclohexylphosphino)pinacoloneazine were determined. Diphosphinoazine ligands in the complexes remained in (Z,Z) configuration bridging two RhCl(C8H12) units.

  • Czech name

    Difosfinoazinové komplexy rhodia(I) a iridia(I)

  • Czech description

    Štěpením můstku chloro(cyclookta-1,5-dien)rhodného dimeru byly připraveny první komplexy rhodia s difosfinoaziny [{RhCl(1,2-h:5,6-h- CH=CHCH2CH2CH=CHCH2CH2 )}2{m-R2PCH2C(But)=NN=C(But)CH2PR2] (R = Ph, Cy, Pri), poprvé byly rovněž připraveny analogické komplexy iridia. Rentgenovou difrakcí byly určeny struktury isostrukturních rhodných a iridných komplexů s bis(dicyklohexylfosfino)pinakolonazinem. Difosfinoazinové ligandy v komplexech zůstávají v (Z,Z) konfiguraci a můstkují dvě RhCl(C8H12) jednotky.

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CC - Organic chemistry

  • OECD FORD branch

Result continuities

  • Project

    Result was created during the realization of more than one project. More information in the Projects tab.

  • Continuities

    Z - Vyzkumny zamer (s odkazem do CEZ)

Others

  • Publication year

    2006

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Collection of Czechoslovak Chemical Communications

  • ISSN

    0010-0765

  • e-ISSN

  • Volume of the periodical

    71

  • Issue of the periodical within the volume

    2

  • Country of publishing house

    CZ - CZECH REPUBLIC

  • Number of pages

    10

  • Pages from-to

    197-206

  • UT code for WoS article

  • EID of the result in the Scopus database