Copper-mediated Synthesis of Mono- and Dichlorinated Diaryl Ethers

Result code in IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F67985858%3A_____%2F14%3A00429530" target="_blank" >RIV/67985858:_____/14:00429530 - isvavai.cz</a>

Result on the web

<a href="http://dx.doi.org/10.1016/j.tetlet.2014.06.035" target="_blank" >http://dx.doi.org/10.1016/j.tetlet.2014.06.035</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.1016/j.tetlet.2014.06.035" target="_blank" >10.1016/j.tetlet.2014.06.035</a>

Result language

angličtina

Original language name

Copper-mediated Synthesis of Mono- and Dichlorinated Diaryl Ethers

Original language description

An efficient synthesis of polychlorinated diphenyl ethers (PCDEs) using the Cu(OAc)2 catalyzed Chan?Lam coupling reaction is described. A library of all possible mono- and dichlorinated diphenyl ether congeners was prepared and characterized using MS, 1H, and 13C NMR spectroscopy, and Kovats retention indices. Our approach, using the optimized reaction conditions (i.e., reaction temperature, oxidizing atmosphere and base), significantly improves and simplifies the process compared to previously reportedsyntheses.

Czech name

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Czech description

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Type

J_x - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

CEP classification

CC - Organic chemistry

OECD FORD branch

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Project

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Continuities

I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Publication year

2014

Confidentiality

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Name of the periodical

Tetrahedron Letters

ISSN

0040-4039

e-ISSN

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Volume of the periodical

55

Issue of the periodical within the volume

30

Country of publishing house

GB - UNITED KINGDOM

Number of pages

4

Pages from-to

4185-4188

UT code for WoS article

000339128700039

EID of the result in the Scopus database

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