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Considerations on electrolysis in electromembrane extraction of basic drugs

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68081715%3A_____%2F15%3A00448871" target="_blank" >RIV/68081715:_____/15:00448871 - isvavai.cz</a>

  • Result on the web

    <a href="http://www.ce-ce.org/CECE2015/CECE%202015%20proceedings_full.pdf" target="_blank" >http://www.ce-ce.org/CECE2015/CECE%202015%20proceedings_full.pdf</a>

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    Considerations on electrolysis in electromembrane extraction of basic drugs

  • Original language description

    Electrolysis may significantly affect composition and pH values of non-optimized acceptor solutions and have fatal consequences on quantitative EME results for weak and medium strong analytes. Acceptor solutions consisting of high concentrations of weakacids have therefore been proposed as suitable operational solutions for electromembrane extraction (EME) of selected basic drugs. 500 mM formic acid efficiently eliminated the electrolytically produced OH? ions, offered constant pH and thus long-term EME performance and was easily compatible with subsequent analytical methods. Maximum EME recoveries ranged from 66 to 89% and were constant between 40 and 80 min of EME and no back-extraction of the analytes into donor solutions was observed.

  • Czech name

  • Czech description

Classification

  • Type

    D - Article in proceedings

  • CEP classification

    CB - Analytical chemistry, separation

  • OECD FORD branch

Result continuities

  • Project

    <a href="/en/project/GA13-05762S" target="_blank" >GA13-05762S: Theory, methodology and development of progressive chemical methods for analysis of trace components and complex samples by capillary electrophoresis.</a><br>

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2015

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Article name in the collection

    CECE 2015. 12th International Interdisciplinary Meeting on Bioanalysis

  • ISBN

    978-80-904959-3-7

  • ISSN

  • e-ISSN

  • Number of pages

    4

  • Pages from-to

    198-201

  • Publisher name

    Ústav analytické chemie AV ČR, v. v. i

  • Place of publication

    Brno

  • Event location

    Brno

  • Event date

    Sep 21, 2015

  • Type of event by nationality

    WRD - Celosvětová akce

  • UT code for WoS article