Enhancing the efficiency of chemical vapor generation of zinc in a multimode sample introduction system
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68081715%3A_____%2F24%3A00588559" target="_blank" >RIV/68081715:_____/24:00588559 - isvavai.cz</a>
Alternative codes found
RIV/00216208:11310/24:10495997
Result on the web
<a href="https://hdl.handle.net/11104/0355419" target="_blank" >https://hdl.handle.net/11104/0355419</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1007/s00706-024-03241-0" target="_blank" >10.1007/s00706-024-03241-0</a>
Alternative languages
Result language
angličtina
Original language name
Enhancing the efficiency of chemical vapor generation of zinc in a multimode sample introduction system
Original language description
Chemical vapor generation (CVG) of Zn was carried out in a multimode sample introduction system (MSIS) and coupled to inductively coupled plasma mass spectrometry (ICP-MS) for detection. CVG conditions were studied and 0.4% (m/v) 8-hydroxyquinoline as the reaction modifier in 0.08 mol dm-3 H2SO4 and 3.0% NaBH4 in 0.1 mol dm-3 NaOH were found optimal, providing the limits of detection and quantification of 2.8 ng cm-3 and 9.3 ng cm-3, respectively. The overall CVG efficiency of 5.3 +/- 0.1% was determined from comparison with solution nebulization-ICP-MS, while 5.7 +/- 0.1% was determined using 65Zn radiotracer and radiometry. The developed methodology was verified by determination of Zn in the standard reference material of fresh water (NIST 1643f). Interference study conducted with 13 hydride-forming and transition elements did not prove ability of any of the tested element to further increase the CVG efficiency, but at the same time, none of them exhibited serious interference except Ag.
Czech name
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Czech description
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Classification
Type
J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database
CEP classification
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OECD FORD branch
10406 - Analytical chemistry
Result continuities
Project
<a href="/en/project/GJ19-17604Y" target="_blank" >GJ19-17604Y: Novel analytical approaches for determination of transition metals based on volatile species generation and atomic fluorescence spectrometry</a><br>
Continuities
I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace
Others
Publication year
2024
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
Monatshefte fur Chemie
ISSN
0026-9247
e-ISSN
1434-4475
Volume of the periodical
155
Issue of the periodical within the volume
8-9
Country of publishing house
DE - GERMANY
Number of pages
9
Pages from-to
889-897
UT code for WoS article
001285909300001
EID of the result in the Scopus database
2-s2.0-85200694012