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Au-Ni nanoparticles: Phase diagram prediction, synthesis, characterization, and thermal stability

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68081723%3A_____%2F17%3A00479236" target="_blank" >RIV/68081723:_____/17:00479236 - isvavai.cz</a>

  • Alternative codes found

    RIV/00216224:14310/17:00094748

  • Result on the web

    <a href="http://dx.doi.org/10.1016/j.calphad.2017.05.002" target="_blank" >http://dx.doi.org/10.1016/j.calphad.2017.05.002</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.calphad.2017.05.002" target="_blank" >10.1016/j.calphad.2017.05.002</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Au-Ni nanoparticles: Phase diagram prediction, synthesis, characterization, and thermal stability

  • Original language description

    The Au-Ni nanoparticles (NPs) were prepared by oleylamine solvothermal synthesis from metal precursors. The Au-Ni phase diagram prediction respecting the particle size was calculated by the CALPHAD method. The hydrodynamic size of the AuNi NPs in a nonpolar organic solvent was measured by the dynamic light scattering (DLS) method. The average hydrodynamic sizes of the nanoparticle samples were between 18 and 25 nm. The metallic composition of the AuNi NP samples was obtained by inductively-coupled plasma atomic emission spectroscopy (ICP-OES). The metallic fraction inside AuNi NPs was varied Au-(30-70) wt%Ni. The steric alkylamine stabilization was observed. The individual AuNi NPs were investigated by transmission electron microscopy (TEM). The dry nanopowder was also studied. The structures of the aggregated samples were investigated by scanning electron microscopy (SEM). The AuNi NPs reveal randomly mixed face-centered cubic (FCC) crystal lattices. The phase transformations were studied under inert gas and air. The samples were studied by differential scanning calorimetry (DSC).

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    20303 - Thermodynamics

Result continuities

  • Project

    Result was created during the realization of more than one project. More information in the Projects tab.

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2017

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Calphad - Computer Coupling of Phase Diagrams and Thermochemistry

  • ISSN

    0364-5916

  • e-ISSN

  • Volume of the periodical

    58

  • Issue of the periodical within the volume

    SEP

  • Country of publishing house

    GB - UNITED KINGDOM

  • Number of pages

    9

  • Pages from-to

    25-33

  • UT code for WoS article

    000410869300004

  • EID of the result in the Scopus database

    2-s2.0-85019063262