Sonochemical synthesis and characterization of nano-sized copper(I) thiosemicarbazone complex: crystal structure and thermal study

Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68378271%3A_____%2F19%3A00519071" target="_blank" >RIV/68378271:_____/19:00519071 - isvavai.cz</a>
Result on the web
<a href="https://doi.org/10.1007/s13738-019-01592-8" target="_blank" >https://doi.org/10.1007/s13738-019-01592-8</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1007/s13738-019-01592-8" target="_blank" >10.1007/s13738-019-01592-8</a>

Result language
angličtina
Original language name
Sonochemical synthesis and characterization of nano-sized copper(I) thiosemicarbazone complex: crystal structure and thermal study
Original language description
In this work, we report the synthesis, characterization, crystal structure, and thermal and antibacterial studies of a new nano-sized copper(I) thiosemicarbazone complex prepared by an ultrasonic bath assisted synthesis in an acetonitrile solution. Characterization of the complex and its ligand (EHB-tsc = 3-ethoxy--hydroxybenzaldehyde-thiosemicarbazone) was performed using elemental analysis, FT-IR, 1H and 13C-NMR, UV–Vis spectroscopy, thermal gravimetry, and singlecrystal X-ray diffraction. In addition, the complex was characterized by X-ray powder diffraction and scanning electron microscopy.
Czech name
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Czech description
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Type
J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database
CEP classification
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OECD FORD branch
10302 - Condensed matter physics (including formerly solid state physics, supercond.)

Project
Result was created during the realization of more than one project. More information in the Projects tab.
Continuities
P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Publication year
2019
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

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