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Crystal structure of vyacheslavite, U(PO4)(OH), solved from natural nanocrystal: a precession electron diffraction tomography (PEDT) study and DFT calculations

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68378271%3A_____%2F19%3A00519120" target="_blank" >RIV/68378271:_____/19:00519120 - isvavai.cz</a>

  • Result on the web

    <a href="http://hdl.handle.net/11104/0304141" target="_blank" >http://hdl.handle.net/11104/0304141</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1039/c9ra03694f" target="_blank" >10.1039/c9ra03694f</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Crystal structure of vyacheslavite, U(PO4)(OH), solved from natural nanocrystal: a precession electron diffraction tomography (PEDT) study and DFT calculations

  • Original language description

    The crystal structure of the U(IV)-phosphate mineral vyacheslavite has been solved from precession electron diffraction tomography (PEDT) data from the natural nano-crystal and further refined using densityfunctional theory (DFT) calculations. Vyacheslavite is orthorhombic, with the space group Cmca. Its structure is a complex heteropolyhedral framework consisting of sheets of UO7(OH) and PO4 polyhedra, running parallel to (001), interconnected by additional PO4 polyhedra. There is an (OH) group associated with the U(IV) polyhedron. The question of H2O presence within the small cavities of the framework has been addressed by the DFT calculations, which have proved that vyacheslavite does not contain any significant amount of H2O at room temperature.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10302 - Condensed matter physics (including formerly solid state physics, supercond.)

Result continuities

  • Project

    <a href="/en/project/GA17-09161S" target="_blank" >GA17-09161S: Crystal structures, chemistry and stability of arsenate and sulfate minerals</a><br>

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2019

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    RSC Advances

  • ISSN

    2046-2069

  • e-ISSN

  • Volume of the periodical

    9

  • Issue of the periodical within the volume

    34

  • Country of publishing house

    GB - UNITED KINGDOM

  • Number of pages

    5

  • Pages from-to

    19657-19661

  • UT code for WoS article

    000475455200042

  • EID of the result in the Scopus database

    2-s2.0-85068231593