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Microstructure and micromechanical properties of GaV4S8 ceramics prepared by single-step solid state synthesis

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68378271%3A_____%2F20%3A00532121" target="_blank" >RIV/68378271:_____/20:00532121 - isvavai.cz</a>

  • Alternative codes found

    RIV/68407700:21340/20:00339676

  • Result on the web

    <a href="https://doi.org/10.1016/j.ceramint.2019.11.194" target="_blank" >https://doi.org/10.1016/j.ceramint.2019.11.194</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.ceramint.2019.11.194" target="_blank" >10.1016/j.ceramint.2019.11.194</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Microstructure and micromechanical properties of GaV4S8 ceramics prepared by single-step solid state synthesis

  • Original language description

    Despite the current focus on the electronic properties of GaV4S8 lacunar spinel, the microstructural and mechanical characterization of this material is scarce in the literature. In this work, we propose an effective GaV4S8 ceramics production method and provide a detailed microstructural and micromechanical characterization. Light microscopy, scanning electron microscopy and X-ray diffraction are used to describe the microstructure of the ceramic targets that can be used for thin film deposition. V2O3 was found to be the main impurity in ceramic targets and its content is discussed with respect to the sintering atmosphere control. Nanoindentation and microcantilever bending were employed to provide estimates of the indentation modulus, hardness and fracture stress of individual grains. The values of these parameters have been determined as Er = 130 ± 2 GPa, H = 8.9 ± 0.2 GPa and σc = 600 ± 57 MPa, respectively.n

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10302 - Condensed matter physics (including formerly solid state physics, supercond.)

Result continuities

  • Project

    Result was created during the realization of more than one project. More information in the Projects tab.

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2020

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Ceramics International

  • ISSN

    0272-8842

  • e-ISSN

  • Volume of the periodical

    46

  • Issue of the periodical within the volume

    6

  • Country of publishing house

    GB - UNITED KINGDOM

  • Number of pages

    5

  • Pages from-to

    7045-7049

  • UT code for WoS article

    000519661800007

  • EID of the result in the Scopus database

    2-s2.0-85075889368