The effect of calcination temperature on the morphology, size and the crystalline phase of the As-synthesized products by direct calcination of FeSO4 at the presence of benzoic acid

Result code in IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68378271%3A_____%2F20%3A00537562" target="_blank" >RIV/68378271:_____/20:00537562 - isvavai.cz</a>

Result on the web

<a href="https://doi.org/10.1134/S1027451020060051" target="_blank" >https://doi.org/10.1134/S1027451020060051</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.1134/S1027451020060051" target="_blank" >10.1134/S1027451020060051</a>

Result language

angličtina

Original language name

The effect of calcination temperature on the morphology, size and the crystalline phase of the As-synthesized products by direct calcination of FeSO4 at the presence of benzoic acid

Original language description

In this paper, we decomposed the FeSO4 at the presence of benzoic acid with weight ratio 1 : 1 at two different temperatures 500 and 600°C. The as-synthesized products were characterized by Fourier Transform Infrared (FT-IR) spectroscopy, powder X-ray diffraction (XRD) and transmission electron microscopy (TEM). FT-IR and XRD results confirmed that the as-prepared product at 500°C is a mixture of intermediate compounds, while the as-prepared product at 600°C is obviously pure with high degree of crystallinity of hematite (α-Fe2O3) nanoparticles. TEM images show that shape, size and morphology of the as-prepared products depend on the calcination temperature.n

Czech name

—

Czech description

—

Type

J_imp - Article in a specialist periodical, which is included in the Web of Science database

CEP classification

—

OECD FORD branch

10302 - Condensed matter physics (including formerly solid state physics, supercond.)

Project

Result was created during the realization of more than one project. More information in the Projects tab.

Continuities

I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Publication year

2020

Confidentiality

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Name of the periodical

Journal of Surface Investigation-X-Ray Synchrotron and Neutron Techniques

ISSN

1027-4510

e-ISSN

—

Volume of the periodical

14

Issue of the periodical within the volume

6

Country of publishing house

RU - RUSSIAN FEDERATION

Number of pages

4

Pages from-to

1191-1195

UT code for WoS article

000603321400014

EID of the result in the Scopus database

2-s2.0-85098273637