Reaction monitoring of cementing materials through multivariate techniques applied to time-resolved synchrotron X-Ray diffraction data
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68378297%3A_____%2F15%3A00452611" target="_blank" >RIV/68378297:_____/15:00452611 - isvavai.cz</a>
Result on the web
<a href="http://www.aidic.it/cet/15/43/150.pdf" target="_blank" >http://www.aidic.it/cet/15/43/150.pdf</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.3303/CET1543150" target="_blank" >10.3303/CET1543150</a>
Alternative languages
Result language
angličtina
Original language name
Reaction monitoring of cementing materials through multivariate techniques applied to time-resolved synchrotron X-Ray diffraction data
Original language description
In this work, the setting reaction of magnesium potassium phosphate ceramic (MKPC) from magnesia (MgO) and potassium di-hydrogen phosphate was investigated by means of in-situ synchrotron X-ray powder diffraction (XRPD). The experimental data were analyzed through multivariate statistical techniques that enabled a real time and reliable understanding of the phenomena occurring in the process. Here, a method combining Multivariate Curve Resolution-Alternating Least Squares (MCR-ALS) with Evolving FactorAnalysis (EFA) was proposed. Comparison with the conventional methods showed that the compounds involved in the process can be correctly distinguished and the main reaction steps, such as reactants consumption, occurrence of intermediate amorphous phaseand MKPC formation can be clearly identified.
Czech name
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Czech description
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Classification
Type
J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)
CEP classification
AN - Psychology
OECD FORD branch
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Result continuities
Project
<a href="/en/project/LO1219" target="_blank" >LO1219: Sustainable advanced development of CET</a><br>
Continuities
P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)
Others
Publication year
2015
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
Chemical Engineering Transactions
ISSN
2283-9216
e-ISSN
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Volume of the periodical
43
Issue of the periodical within the volume
May
Country of publishing house
IT - ITALY
Number of pages
6
Pages from-to
895-900
UT code for WoS article
000365994200150
EID of the result in the Scopus database
2-s2.0-84946080121