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Soft magnetic amorphous alloys in X-ray light: Insights from ultra-fast Joule heating experiments

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F68407700%3A21340%2F20%3A00337606" target="_blank" >RIV/68407700:21340/20:00337606 - isvavai.cz</a>

  • Result on the web

    <a href="https://doi.org/10.1016/j.jmmm.2019.166282" target="_blank" >https://doi.org/10.1016/j.jmmm.2019.166282</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.jmmm.2019.166282" target="_blank" >10.1016/j.jmmm.2019.166282</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Soft magnetic amorphous alloys in X-ray light: Insights from ultra-fast Joule heating experiments

  • Original language description

    In this contribution a novel setup for studying rapid crystallization of metallic glasses using a time resolved in situ X-ray diffraction combined with a direct current fast Joule heating (flash-annealing) is presented. The setup was implemented and successfully tested at the P02.1 beamline of the PETRA III storage ring (DESY Hamburg, Germany). Its potential use is demonstrated by studying rapid crystallization of soft magnetic Fe73.5Cu1Nb3Si15.5B7 (at.%) metallic glass prepared by melt spinning technique. Flash-annealing experiment is realized by bursting 20 rectangular current pulses with a fixed amplitude of 1.5 A and pulse length δ is varied (30, 40 and 50 ms). A single pulse with duration of 30 ms causes temperature to rise to 770 °C with an average heating rate of 4200 K/s. Phase composition of crystallized material consist of major Fe3Si phase and small traces of boride phase Fe23B6. Consecutive pulses result in cyclic thermal expansion of a crystal lattice, which appears fully reversible. Increasing pulse width to 50 ms causes temperature to increase up to 1020 °C with an average heating rate of 5600 K/s. Differentiation of the temperature profile yields exceptionally high value of heating rate 10800 ± 2400 K/s.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    20501 - Materials engineering

Result continuities

  • Project

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2020

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Journal of Magnetism and Magnetic Materials

  • ISSN

    0304-8853

  • e-ISSN

    1873-4766

  • Volume of the periodical

    499

  • Issue of the periodical within the volume

    166282

  • Country of publishing house

    NL - THE KINGDOM OF THE NETHERLANDS

  • Number of pages

    4

  • Pages from-to

  • UT code for WoS article

    000510014100056

  • EID of the result in the Scopus database

    2-s2.0-85076424052