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Curing behavior and reaction kinetics of binder resins for 3D-printing investigated by dielectric analysis (DEA)

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F70883521%3A28610%2F16%3A43874637" target="_blank" >RIV/70883521:28610/16:43874637 - isvavai.cz</a>

  • Result on the web

    <a href="http://aip.scitation.org/doi/abs/10.1063/1.4949649" target="_blank" >http://aip.scitation.org/doi/abs/10.1063/1.4949649</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1063/1.4949649" target="_blank" >10.1063/1.4949649</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Curing behavior and reaction kinetics of binder resins for 3D-printing investigated by dielectric analysis (DEA)

  • Original language description

    3D-Printing is an efficient method in the field of additive manufacturing. In order to optimize the properties of manufactured parts it is essential to adapt the curing behavior of the resin systems with respect to the requirements. Thus, effects of resin composition, e.g. due to different additives such as thickener and curing agents, on the curing behavior have to be known. As the resin transfers from a liquid to a solid glass the time dependent ion viscosity was measured using DEA with flat IDEX sensors. This allows for a sensitive measurement of resin changes as the ion viscosity changes two to four decades. The investigated resin systems are based on the monomers styrene and HEMA. To account for the effects of copolymerization in the calculation of the reaction kinetics it was assumed that the reaction can be considered as a homo-polymerization having a reaction order n?1. Then the measured ion viscosity curves are fitted with the solution of the reactions kinetics - the time dependent degree of conversion (DC-function) - for times exceeding the initiation phase representing the primary curing. The measured ion viscosity curves can nicely be fitted with the DC-function and the determined fit parameters distinguish distinctly between the investigated resin compositions.

  • Czech name

  • Czech description

Classification

  • Type

    D - Article in proceedings

  • CEP classification

    CD - Macromolecular chemistry

  • OECD FORD branch

Result continuities

  • Project

  • Continuities

    N - Vyzkumna aktivita podporovana z neverejnych zdroju

Others

  • Publication year

    2016

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Article name in the collection

    Proceedings of PPS-30: The 30th International Conference of the Polymer Processing Society

  • ISBN

    978-0-7354-1309-2

  • ISSN

    0094-243X

  • e-ISSN

  • Number of pages

    4

  • Pages from-to

  • Publisher name

    American Institute of Physics

  • Place of publication

    Melville

  • Event location

    Ischia

  • Event date

    Jun 19, 2016

  • Type of event by nationality

    WRD - Celosvětová akce

  • UT code for WoS article