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Spectroscopic characterisation of Naples yellow variations in paintings from the turn of the 20th century

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00007064%3AK01__%2F22%3AN0000121" target="_blank" >RIV/00007064:K01__/22:N0000121 - isvavai.cz</a>

  • Alternative codes found

    RIV/00023281:_____/22:N0000048 RIV/00216275:25310/23:39919308

  • Result on the web

    <a href="https://analyticalsciencejournals.onlinelibrary.wiley.com/doi/10.1002/jrs.6470" target="_blank" >https://analyticalsciencejournals.onlinelibrary.wiley.com/doi/10.1002/jrs.6470</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1002/jrs.6470" target="_blank" >10.1002/jrs.6470</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Spectroscopic characterisation of Naples yellow variations in paintings from the turn of the 20th century

  • Original language description

    The research presented in this study aimed to document the variability of synthetic lead antimonate pigments known as Naples yellow in selected artworks by Czech landscape painters from the turn of the 20th century. Spectra obtained through Raman spectroscopy show considerable difference in the position of main band maximum (from 110 to 145 cm(-1)) characteristic of cubic pyrochlore structure Pb2Sb2O7-the major phase of the Naples yellow pigment. In several samples, hexagonal PbSb2O6 with main band at 655 cm(-1) was identified as a dominant phase, a finding that is somewhat surprising because PbSb2O6 has been generally considered a minor admixture to cubic Pb2Sb2O7. Reference pigment samples were synthesised under known conditions, and their spectra were collected in order to get more comparative material. Also, commercially available Naples yellow pigments were characterised in the same way. We observed considerable differences of the obtained spectra caused by the presence of admixtures and diverse production conditions. The diversity of Naples yellow and the corresponding Raman spectra makes their identification problematic. Presented data thus may serve as a reference material in the identification process.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    50902 - Social sciences, interdisciplinary

Result continuities

  • Project

    <a href="/en/project/VJ01010004" target="_blank" >VJ01010004: The Development of a Strategic Cluster for Effective Instrumental Technological Methods of Forensic Authentication of Modern Artworks</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2022

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    https://analyticalsciencejournals.onlinelibrary.wiley.com/journal/10974555

  • ISSN

    0377-0486

  • e-ISSN

    1097-4555

  • Volume of the periodical

    54

  • Issue of the periodical within the volume

    2

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    11

  • Pages from-to

    171-181

  • UT code for WoS article

    000888463600001

  • EID of the result in the Scopus database

    2-s2.0-85142416170