The role of silver nanoparticles synthesized from Brassica olerace for determination of Aspirin in pharmaceutical samples by standard additions method
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216208%3A11140%2F23%3A10483273" target="_blank" >RIV/00216208:11140/23:10483273 - isvavai.cz</a>
Result on the web
<a href="https://verso.is.cuni.cz/pub/verso.fpl?fname=obd_publikace_handle&handle=t7WimPahkd" target="_blank" >https://verso.is.cuni.cz/pub/verso.fpl?fname=obd_publikace_handle&handle=t7WimPahkd</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.56053/7.2.95" target="_blank" >10.56053/7.2.95</a>
Alternative languages
Result language
angličtina
Original language name
The role of silver nanoparticles synthesized from Brassica olerace for determination of Aspirin in pharmaceutical samples by standard additions method
Original language description
In this study, silver nanoparticles (Ag NPs) were prepared from Brassica oleracea (BO) leaflet extract (BO-AgNPs) and applied for to determination of Aspirin in pharmaceutical samples through selective and sensitive spectrophotometric standard additions method. The measurements of UV-Visible, X-ray diffraction (XRD), Fourier transform infrared (FTIR) and scanning electron microscopy (SEM) have been used to confirm the formation of BO-AgNPs, revealing a prominent absorption band at 450 nm, crystallinity, and an agglomerated morphology having an average particle size of 29 nm. Aspirin in Acifein, Aspirin, Acylpyrin and Disprin tablets was determined through the complexation with BO-AgNPs, revealing a linear range of 1-10 mg/10 mL and limit of detection (LOD) as 0.09, 0.46, 0.69 and 0.99 mg/10 mL, respectively. An average percent recovery for four samples were found to be 90, 99, 101 and 99 % and relative standard deviation (RSD) as 1.6, 0.6, 0.3 and 1.4, respectively. The suggested method was successfully used for the quantitative analysis of pharmaceutical tablets, which opens up the possibility that Ag NPs could be used to determine biological molecules when interferences from real samples are present.
Czech name
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Czech description
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Classification
Type
J<sub>SC</sub> - Article in a specialist periodical, which is included in the SCOPUS database
CEP classification
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OECD FORD branch
30104 - Pharmacology and pharmacy
Result continuities
Project
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Continuities
I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace
Others
Publication year
2023
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
Experimental and Theoretical Nanotechnology
ISSN
2590-4132
e-ISSN
2590-4132
Volume of the periodical
7
Issue of the periodical within the volume
2
Country of publishing house
DZ - THE PEOPLE'S DEMOCRATIC REPUBLIC OF ALGERIA
Number of pages
16
Pages from-to
95-110
UT code for WoS article
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EID of the result in the Scopus database
2-s2.0-85200961355