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Crystallization and characterization of the compounds Gly.MSO4.mH2O (M = Mg2+, Mn2+, Fe2+, Co2+, Ni2+, Zn2+; m = 0, 3, 5, 6)

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216208%3A11310%2F12%3A10127269" target="_blank" >RIV/00216208:11310/12:10127269 - isvavai.cz</a>

  • Alternative codes found

    RIV/61388980:_____/12:00377358

  • Result on the web

    <a href="http://dx.doi.org/10.1016/j.molstruc.2012.02.068" target="_blank" >http://dx.doi.org/10.1016/j.molstruc.2012.02.068</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.molstruc.2012.02.068" target="_blank" >10.1016/j.molstruc.2012.02.068</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Crystallization and characterization of the compounds Gly.MSO4.mH2O (M = Mg2+, Mn2+, Fe2+, Co2+, Ni2+, Zn2+; m = 0, 3, 5, 6)

  • Original language description

    The equilibrium crystallization of complex compounds of the type Gly.MSO4.5H2O with a structure derived from those of the crystallized double salts MSO4.xH2O, where x = 6, 7 was predicted and proven in the systems Gly-MSO4-H2O (M = Mg2+, Mn2+, Fe2+, Co2+, Ni2+ and Zn2+). It was predicted that stable octahedral complexes [M(H2O)6]2+ and trans-[M(H2O)4(O-gly)2]2+, as well as [SO4]2MINUS SIGN tetrahedra, which were the main building units of the crystallizing Gly.MSO4.5H2O compounds (triclinic crystal system, space group P MINUS SIGN 1), were predominating in these solutions. The vibrational spectra and the thermal behavior of the Gly.MSO4.5H2O compounds (M = Mg2+, Co2+, Zn2+) are in accord with the refined crystal structures. The cobalt compound displaysantiferromagnetic behavior whereas the nickel and manganese compounds are ferromagnetic. In the manganese system where MnSO4.H2O (308 K) crystallizes, the only complex compound is the anhydrous Gly.MnSO4 with a polymeric type structure .

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CA - Inorganic chemistry

  • OECD FORD branch

Result continuities

  • Project

    <a href="/en/project/GA203%2F09%2F0878" target="_blank" >GA203/09/0878: Crystal engineering of hydrogen bonded materials for non-linear optics</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)<br>Z - Vyzkumny zamer (s odkazem do CEZ)<br>I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2012

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Journal of Molecular Structure

  • ISSN

    0022-2860

  • e-ISSN

  • Volume of the periodical

    1018

  • Issue of the periodical within the volume

    březen

  • Country of publishing house

    NL - THE KINGDOM OF THE NETHERLANDS

  • Number of pages

    9

  • Pages from-to

    113-121

  • UT code for WoS article

    000305847100019

  • EID of the result in the Scopus database