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The Effect of Synthesis Conditions and Nature of Heteroelement on Acidic Properties of Isomorphously Substituted UTL Zeolites

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216208%3A11310%2F13%3A10134296" target="_blank" >RIV/00216208:11310/13:10134296 - isvavai.cz</a>

  • Alternative codes found

    RIV/61388955:_____/13:00392940

  • Result on the web

    <a href="http://dx.doi.org/10.1166/apm.2013.1011" target="_blank" >http://dx.doi.org/10.1166/apm.2013.1011</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1166/apm.2013.1011" target="_blank" >10.1166/apm.2013.1011</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    The Effect of Synthesis Conditions and Nature of Heteroelement on Acidic Properties of Isomorphously Substituted UTL Zeolites

  • Original language description

    The possibility to modify the acidic properties of extra-large pore UTL zeolite, possessing unique two-dimensional 14- and 12-ring pore system, was evidenced. Acid strength increases in order B-UTL<Fe-UTL<Ga-UTL<Al-UTL and the concentration of Bronsted acid centers in Al-, Ga-, and Fe-UTL frameworks could be adjusted by changing the pH value of the initial gel. The acidic properties of isomorphously substituted UTL zeolites with different heteroelements (B, Al, Ga, Fe) in the framework, were investigated using FTIR of adsorbed pyridine, ammonia temperature programmed desorption (TPD of NH3 and Hammett indicator method. Pure germanosilicate UTL zeolites contain two types of acid centers: (i) weak silanol and germanol groups with strength 48<H0 < 68 (characterized by the band at 1446 cmMINUS SIGN 1 in IR spectra of adsorbed pyridine and by desorption peak at 180 C in TPD of NH3 and (ii) Lewis acid centers attributed to 4-coordinated Ge with strength MINUS SIGN 82 < H0 < MINUS SIGN 56 (ch

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CF - Physical chemistry and theoretical chemistry

  • OECD FORD branch

Result continuities

  • Project

    Result was created during the realization of more than one project. More information in the Projects tab.

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2013

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    ADVANCED POROUS MATERIALS

  • ISSN

    2327-3941

  • e-ISSN

  • Volume of the periodical

    1

  • Issue of the periodical within the volume

    1

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    11

  • Pages from-to

    103-113

  • UT code for WoS article

  • EID of the result in the Scopus database