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Dissociation kinetics study of copper(II) complexes of DO3A, DOTA and its monosubstituted derivatives

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216208%3A11310%2F13%3A10139599" target="_blank" >RIV/00216208:11310/13:10139599 - isvavai.cz</a>

  • Alternative codes found

    RIV/00216224:14740/13:00066398

  • Result on the web

    <a href="http://dx.doi.org/10.1016/j.poly.2013.05.042" target="_blank" >http://dx.doi.org/10.1016/j.poly.2013.05.042</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.poly.2013.05.042" target="_blank" >10.1016/j.poly.2013.05.042</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Dissociation kinetics study of copper(II) complexes of DO3A, DOTA and its monosubstituted derivatives

  • Original language description

    The kinetic inertness of copper(II) complexes with cyclen-based ligands having three (H3do3a) or four (H4dota) acetic acid arms and those with 3 acetic acid and one phosphonic (H5do3ap), phosphinic (H5do3ap(PrA) , H4do3ap(ABn)) acid or methylpyridine-N-oxide (H3do3a-pyNox) pendant arms has been studied. The proton-assisted decomplexation reaction was studied under a wide range of conditions to fully assess the parameters influencing the reaction (temperature range 25-60 oC, proton concentration range 0.05-5 M and presence of perchlorate or nitrate anions). The empirical rate law k(d,obs) = k(0) + k(H) x [H+], involving solvolytic and proton-assisted dissociation pathways, shows that the complexes can be divided into two groups according to their kinetic behavior. Complexes of ligands having only carboxylate pendant arms (H3do3a, H4dota) show higher kinetic inertness than those of ligands with mixed pendant arms (H5do3ap, H5do3ap(PrA), H4do3ap(ABn), H3do3a-pyNox). Linear Free Energy Rel

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CA - Inorganic chemistry

  • OECD FORD branch

Result continuities

  • Project

    Result was created during the realization of more than one project. More information in the Projects tab.

  • Continuities

    Z - Vyzkumny zamer (s odkazem do CEZ)<br>I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2013

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Polyhedron

  • ISSN

    0277-5387

  • e-ISSN

  • Volume of the periodical

    61

  • Issue of the periodical within the volume

    September

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    6

  • Pages from-to

    99-104

  • UT code for WoS article

    000322938100014

  • EID of the result in the Scopus database