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Determination of antibiotics in in?uents and e?uents of wastewater-treatment-plants in the Czech Republic - development and application of the SPE and a UHPLC-ToFMS method

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216208%3A11310%2F13%3A10144181" target="_blank" >RIV/00216208:11310/13:10144181 - isvavai.cz</a>

  • Result on the web

    <a href="http://dx.doi.org/10.1039/c3ay00048f" target="_blank" >http://dx.doi.org/10.1039/c3ay00048f</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1039/c3ay00048f" target="_blank" >10.1039/c3ay00048f</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Determination of antibiotics in in?uents and e?uents of wastewater-treatment-plants in the Czech Republic - development and application of the SPE and a UHPLC-ToFMS method

  • Original language description

    A method consisting of solid phase extraction followed by ultra-high performance liquid chromatography combined with time-of-flight mass spectrometry (UHPLC-ToFMS) has been developed for the determination of multiple-class antibiotics in influents and effluents of wastewater-treatment-plants (WWTPs). The nineteen analyzed antibiotics belong to the 5 most prescribed antibiotic classes in the Czech Republic, namely tetracyclines, macrolides, sulfonamides, fluoroquinolones, and lincosamides. The matrix-matched calibration technique with internal standard addition for each antibiotic group was employed for quantification. Two extractions employing an Oasis HLB cartridge and two injections were needed for each sample due to the different physico-chemical properties of the tested antibiotics. Prior to the extraction on the Oasis HLB SPE cartridge, the samples were adjusted to pH 4.5 and 7.5. The usefulness and versatility of the method was documented by achieving method limits of quantificat

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CB - Analytical chemistry, separation

  • OECD FORD branch

Result continuities

  • Project

    <a href="/en/project/1M06011" target="_blank" >1M06011: The Centre of Molecular Methods for Monitoring the Diffuse Pollution of the Environment.</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)<br>Z - Vyzkumny zamer (s odkazem do CEZ)<br>S - Specificky vyzkum na vysokych skolach<br>I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2013

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Analytical Methods

  • ISSN

    1759-9660

  • e-ISSN

  • Volume of the periodical

    5

  • Issue of the periodical within the volume

    8

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    9

  • Pages from-to

    2110-2118

  • UT code for WoS article

    000316960200031

  • EID of the result in the Scopus database