Determination of antibiotics in influents and effluents of wastewater-treatment-plants in the Czech Republic ? development and application of the SPE and a UHPLC-ToFMS method
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F61388971%3A_____%2F13%3A00395780" target="_blank" >RIV/61388971:_____/13:00395780 - isvavai.cz</a>
Alternative codes found
RIV/60193697:_____/13:#0000831
Result on the web
<a href="http://dx.doi.org/10.1039/c3ay00048f" target="_blank" >http://dx.doi.org/10.1039/c3ay00048f</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1039/c3ay00048f" target="_blank" >10.1039/c3ay00048f</a>
Alternative languages
Result language
angličtina
Original language name
Determination of antibiotics in influents and effluents of wastewater-treatment-plants in the Czech Republic ? development and application of the SPE and a UHPLC-ToFMS method
Original language description
A method consisting of solid phase extraction followed by ultra-high performance liquid chromatography combined with time-of-flight mass spectrometry (UHPLC-ToFMS) has been developed for the determination of multiple-class antibiotics in influents and effluents of wastewater-treatment-plants (WWTPs). The nineteen analyzed antibiotics belong to the 5 most prescribed antibiotic classes in the Czech Republic, namely tetracyclines, macrolides, sulfonamides, fluoroquinolones, and lincosamides. The matrix-matched calibration technique with internal standard addition for each antibiotic group was employed for quantification. Two extractions employing an Oasis HLB cartridge and two injections were needed for each sample due to the different physico-chemical properties of the tested antibiotics. Prior to the extraction on the Oasis HLB SPE cartridge, the samples were adjusted to pH 4.5 and 7.5. The usefulness and versatility of the method was documented by achieving method limits of quantificat
Czech name
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Czech description
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Classification
Type
J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)
CEP classification
CB - Analytical chemistry, separation
OECD FORD branch
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Result continuities
Project
<a href="/en/project/1M06011" target="_blank" >1M06011: The Centre of Molecular Methods for Monitoring the Diffuse Pollution of the Environment.</a><br>
Continuities
I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace
Others
Publication year
2013
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
Analytical Methods: advancing methods and applications
ISSN
1759-9660
e-ISSN
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Volume of the periodical
5
Issue of the periodical within the volume
8
Country of publishing house
GB - UNITED KINGDOM
Number of pages
9
Pages from-to
2110-2118
UT code for WoS article
000316960200031
EID of the result in the Scopus database
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