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Complexation of DNA with QPDMAEMA-b-PLMA-b-POEGMA Cationic Triblock Terpolymer Micelles

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216208%3A11310%2F20%3A10419519" target="_blank" >RIV/00216208:11310/20:10419519 - isvavai.cz</a>

  • Result on the web

    <a href="https://verso.is.cuni.cz/pub/verso.fpl?fname=obd_publikace_handle&handle=0isX1y.MWX" target="_blank" >https://verso.is.cuni.cz/pub/verso.fpl?fname=obd_publikace_handle&handle=0isX1y.MWX</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1021/acs.macromol.0c00388" target="_blank" >10.1021/acs.macromol.0c00388</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Complexation of DNA with QPDMAEMA-b-PLMA-b-POEGMA Cationic Triblock Terpolymer Micelles

  • Original language description

    In this work, we investigate the formation and structure of complexes between quaternized poly(2-(dimethylamino)ethyl methacrylate-b-lauryl methacrylate-b-(oligo ethylene glycol) methacrylate) (QPDMAEMA-b-PLMA-b-POEGMA) amphiphilic triblock terpolymer micelles, with different compositions, and DNAs of different lengths. In aqueous solutions, the terpolymers self-assemble in spherical micelles comprising hydrophobic PLMA cores and mixed QPDMAEMA/POEGMA coronas. Terpolymer/DNA micelleplexes were prepared in a wide range of amine over phosphate group ratios (N/P), and linear DNA of different lengths (2000 base pairs and 113 base pairs) was utilized. The complexation ability of the polymeric micelles with DNA was studied by UV-vis spectroscopy and ethidium bromide quenching assays using fluorescence spectroscopy. The thermodynamic interactions that take place during complexation were investigated by isothermal titration calorimetry, whereas the structural characteristics of the micelleplexes were determined by lights-cattering techniques (dynamic, static, and electrophoretic) and cryogenic transmission electron microscopy (cryo-TEM) imaging. All terpolymer micelles effectively complex DNAs, forming micelleplexes, with their size, surface charge, and structure depending on the ratio of the components, length of the DNA, and the chemical structure of the terpolymers. Cryo-TEM revealed the clustering of terpolymer micelles due to complexation with the clusters having different topologies influenced remarkably by the length of the DNA utilized.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10404 - Polymer science

Result continuities

  • Project

    <a href="/en/project/LTAIN19078" target="_blank" >LTAIN19078: Stimuli-Responsive Block Copolymer Based Nanostructured Single-/Multi-component Micelles: Materials and Applications</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)<br>I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2020

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Macromolecules

  • ISSN

    0024-9297

  • e-ISSN

  • Volume of the periodical

    53

  • Issue of the periodical within the volume

    14

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    9

  • Pages from-to

    5747-5755

  • UT code for WoS article

    000557761800010

  • EID of the result in the Scopus database

    2-s2.0-85088022590