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Single-crystal vs polycrystalline boron-doped diamond anodes: Comparing degradation efficiencies of carbamazepine in electrochemical water treatment

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216208%3A11310%2F24%3A10487991" target="_blank" >RIV/00216208:11310/24:10487991 - isvavai.cz</a>

  • Result on the web

    <a href="https://verso.is.cuni.cz/pub/verso.fpl?fname=obd_publikace_handle&handle=h3cWQjpkR5" target="_blank" >https://verso.is.cuni.cz/pub/verso.fpl?fname=obd_publikace_handle&handle=h3cWQjpkR5</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.envpol.2024.123705" target="_blank" >10.1016/j.envpol.2024.123705</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Single-crystal vs polycrystalline boron-doped diamond anodes: Comparing degradation efficiencies of carbamazepine in electrochemical water treatment

  • Original language description

    The ongoing challenge of water pollution by contaminants of emerging concern calls for more effective wastewater treatment to prevent harmful side effects to the environment and human health. To this end, this study explored for the first time the implementation of single-crystal boron-doped diamond (BDD) anodes in electrochemical wastewater treatment, which stand out from the conventional polycrystalline BDD morphologies widely reported in the literature. The single-crystal BDD presented a pure diamond (sp(3)) content, whereas the three other investigated polycrystalline BDD electrodes displayed various properties in terms of boron doping, sp(3)/sp(2) content, microstructure, and roughness. The effects of other process conditions, such as applied current density and anolyte concentration, were simultaneously investigated using carbamazepine (CBZ) as a representative target pollutant. The Taguchi method was applied to elucidate the optimal operating conditions that maximised either (i) the CBZ degradation rate constant (enhanced through hydroxyl radicals (.OH) or (ii) the proportion of sulfate radicals (SO4 .-) with respect to (.OH). The results showed that the single-crystal BDD significantly promoted (.OH) formation but also that the interactions between boron doping, current density and anolyte concentration determined the underlying degradation mechanisms. Therefore, this study demonstrated that characterising the BDD material and understanding its interactions with other process operating conditions prior to degradation experiments is a crucial step to attain the optimisation of any wastewater treatment application.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10406 - Analytical chemistry

Result continuities

  • Project

  • Continuities

    S - Specificky vyzkum na vysokych skolach<br>I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2024

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Environmental Pollution

  • ISSN

    0269-7491

  • e-ISSN

    1873-6424

  • Volume of the periodical

    347

  • Issue of the periodical within the volume

    April

  • Country of publishing house

    GB - UNITED KINGDOM

  • Number of pages

    10

  • Pages from-to

    123705

  • UT code for WoS article

    001208777900001

  • EID of the result in the Scopus database

    2-s2.0-85187222201