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Tuning the morphology of sputter-deposited platinum catalyst: From compact layers to dispersed nanoparticles

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216208%3A11320%2F23%3A10468342" target="_blank" >RIV/00216208:11320/23:10468342 - isvavai.cz</a>

  • Result on the web

    <a href="https://verso.is.cuni.cz/pub/verso.fpl?fname=obd_publikace_handle&handle=eaDhh2O5R8" target="_blank" >https://verso.is.cuni.cz/pub/verso.fpl?fname=obd_publikace_handle&handle=eaDhh2O5R8</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.surfin.2023.103079" target="_blank" >10.1016/j.surfin.2023.103079</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Tuning the morphology of sputter-deposited platinum catalyst: From compact layers to dispersed nanoparticles

  • Original language description

    A comprehensive study on adjusting the morphology of sputter-deposited platinum was performed. Platinum was deposited under various Ar pressure ranging from 0.3 to 3.2 Pa using a conventional magnetron system as well as at 57 Pa using a gas aggregation cluster source integrated into the magnetron sputtering system. The morphology and structure of deposited layers were characterized with a broad portfolio of characterization techniques such as scanning electron microscopy, transmission electron microscopy, grazing incidence small angle X-ray scattering and X-ray diffraction. The results revealed a continuous evolution of the Pt layer morphology from a thin-film-like layer of tightly packed Pt nanoparticles to a deposit composed of dispersed particles of 5-7 nm in size as the Ar pressure increased. The electrochemically active surface area of deposited Pt, as calculated from cyclic voltammograms, increased with deposition pressure from 11.7 m(2)center dot g(Pt)(-1) to 22.3 m(2)center dot g(Pt)(-1) and 24 m(2)center dot g(Pt)(-1) for Pt deposited at 0.3, 3.2 and 57 Pa, respectively. This increase in active sites was reflected in a significant improvement in the mass activity of platinum exemplary confirmed using a methanol electrooxidation reaction.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10305 - Fluids and plasma physics (including surface physics)

Result continuities

  • Project

    Result was created during the realization of more than one project. More information in the Projects tab.

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2023

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Surfaces and Interfaces

  • ISSN

    2468-0230

  • e-ISSN

    2468-0230

  • Volume of the periodical

    40

  • Issue of the periodical within the volume

    Aug

  • Country of publishing house

    NL - THE KINGDOM OF THE NETHERLANDS

  • Number of pages

    7

  • Pages from-to

    103079

  • UT code for WoS article

    001058542500001

  • EID of the result in the Scopus database

    2-s2.0-85163012883