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A new route to the syntheses of alkali metal bis(fluorosulfuryl)imides: Crystal structure of LiN(SO2F)2

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216224%3A14310%2F06%3A00016682" target="_blank" >RIV/00216224:14310/06:00016682 - isvavai.cz</a>

  • Alternative codes found

    RIV/68081715:_____/06:00039220

  • Result on the web

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    A new route to the syntheses of alkali metal bis(fluorosulfuryl)imides: Crystal structure of LiN(SO2F)2

  • Original language description

    A new route for the preparation of Li and Na salts of imido-bis(sulfuric acid) difluoride from KN(SO2F)2 as a starting material is described. KN(SO2F)2 was converted to Li and Na salts by metathetical reactions with lithium and sodium perchlorates in acetonitrile, while Rb and Cs salts were obtained from imido-bis(sulfuric acid) difluoride liberated from its K-salt. The crystal structure of lithium bis(fluorosulfuryl) imide LiN(SO2F)2 (LISFI) was determined.

  • Czech name

    Nový způsob přípravy bis(fluorosulfuryl)amidů alkalických kovů. Krystalová struktura LiN(SO2F)2

  • Czech description

    V článku je popsán nový způsob přípravy alkalických solí imidu kyseliny bis(fluorosírové). Draselná sůl byla převedena na lithnou a sodnou reakcí s odpovídajícími chloristany, zatímco Rb a Cs sůl byly připraveny z volného difluoridu kyseliny imido-bis(sírové). Byla určena krystalová struktura lithné soli,LiN(SO2F)2.

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CA - Inorganic chemistry

  • OECD FORD branch

Result continuities

  • Project

  • Continuities

    Z - Vyzkumny zamer (s odkazem do CEZ)

Others

  • Publication year

    2006

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Polyhedron

  • ISSN

    0277-5387

  • e-ISSN

  • Volume of the periodical

    26

  • Issue of the periodical within the volume

    6

  • Country of publishing house

    CZ - CZECH REPUBLIC

  • Number of pages

    7

  • Pages from-to

    1292-1298

  • UT code for WoS article

  • EID of the result in the Scopus database