Determination of polycyclic aromatic nitrogen heterocycles in soil using liquid chromatography/tandem mass spectrometry
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216224%3A14310%2F09%3A00036101" target="_blank" >RIV/00216224:14310/09:00036101 - isvavai.cz</a>
Result on the web
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DOI - Digital Object Identifier
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Alternative languages
Result language
angličtina
Original language name
Determination of polycyclic aromatic nitrogen heterocycles in soil using liquid chromatography/tandem mass spectrometry
Original language description
Development of LC/MS/MS method for analysing polycyclic aromatic nitrogen hydrocarbons (PANHs) in soil samples is presented. Optimisation of individual chromatographic/mass spectrometric conditions was made in order to obtain a method for the determination of 15 PANHs content in an organic extract from the soil. Detection limits (LOD) in the range of 0.3 to 15 pg per injection were 15 obtained for individual PANHs. LC/MS/MS method has a lower LOD value compared to LC/DAD/FLD methods in general. Developed LC/MS/MS method was used for determination of PANHs content in soil samples collected in contaminated areas of the southeast region of the Czech Republic. Highest concentrations of PANHs have been found in the samples collected in the immediate vicinity of the industrial basin. Concentrations of the contaminants in samples collected in surrounding villages were higher compared to the sample collected in clean area of the Czech Republic.
Czech name
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Czech description
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Classification
Type
J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)
CEP classification
CB - Analytical chemistry, separation
OECD FORD branch
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Result continuities
Project
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Continuities
Z - Vyzkumny zamer (s odkazem do CEZ)<br>S - Specificky vyzkum na vysokych skolach
Others
Publication year
2009
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
International Journal of Environmental analytical cemistry
ISSN
0306-7319
e-ISSN
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Volume of the periodical
Vol. 89
Issue of the periodical within the volume
No. 3
Country of publishing house
GB - UNITED KINGDOM
Number of pages
15
Pages from-to
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UT code for WoS article
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EID of the result in the Scopus database
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