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Analysis of alkylphenols and bisphenols in soils using liquid chromatography-tandem mass spectrometry

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216224%3A14310%2F21%3A00118726" target="_blank" >RIV/00216224:14310/21:00118726 - isvavai.cz</a>

  • Alternative codes found

    RIV/60193697:_____/19:N0000049

  • Result on the web

    <a href="https://www.tandfonline.com/doi/full/10.1080/03067319.2019.1679804" target="_blank" >https://www.tandfonline.com/doi/full/10.1080/03067319.2019.1679804</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1080/03067319.2019.1679804" target="_blank" >10.1080/03067319.2019.1679804</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Analysis of alkylphenols and bisphenols in soils using liquid chromatography-tandem mass spectrometry

  • Original language description

    Methods useful for the extraction of alkylphenols from soil samples were assessed. A comparison is made of the four extraction techniques that are most commonly used to extract phenolic compounds from soil, such as bisphenol A, bisphenol F and alkylphenols (4-t-OP, iso-NP, 4-OP and 4-n-NP). Soxhlet extraction, ultrasonic-assisted extraction (USE), accelerated solvent extraction (ASE) and the so-called Quick, Easy, Cheap, Effective, Rugged and Safe extraction (QuEChERS) were included. Modifications of the QuEChERS technique such as original, citrate and acetate were investigated. The effects of basic purification sorbents used for QuEChERS extracts such as a primary and secondary amine (PSA), C18 endcapped sorbents and graphitised carbon black (GCB) were tested. A derivatisation step prior to the final analyses by liquid chromatography coupled to a triple quadrupole analyser operating in tandem mass spectrometry (LC-MS/MS) was performed by using dansyl chloride (DNSC). The best extraction of the monitored compounds from spiked soil was obtained using QuEChERS extraction. Recoveries of phenolic compounds using the QuEChERS technique were in the range from 67% to 114%. The lowest extraction recoveries (16-73%) were obtained using ultrasonic extraction. The QuEChERS method was successfully applied for the analysis of alkylphenols in soil samples. Instrumental limits of quantification and limits of detection ranged from 0.08 to 0.83 pg per injection and 0.02 to 0.25 pg per injection, respectively.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10400 - Chemical sciences

Result continuities

  • Project

    Result was created during the realization of more than one project. More information in the Projects tab.

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2021

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    International Journal of Environmental Analytical Chemistry

  • ISSN

    0306-7319

  • e-ISSN

    1029-0397

  • Volume of the periodical

    101

  • Issue of the periodical within the volume

    9

  • Country of publishing house

    GB - UNITED KINGDOM

  • Number of pages

    15

  • Pages from-to

    1287-1301

  • UT code for WoS article

    000492108700001

  • EID of the result in the Scopus database

    2-s2.0-85074522266