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Multigram preparation of tungsten microfibers via needle-less electrospinning of phosphotungstic acid

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216224%3A14310%2F23%3A00130332" target="_blank" >RIV/00216224:14310/23:00130332 - isvavai.cz</a>

  • Result on the web

    <a href="https://doi.org/10.1016/j.ijrmhm.2023.106121" target="_blank" >https://doi.org/10.1016/j.ijrmhm.2023.106121</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.ijrmhm.2023.106121" target="_blank" >10.1016/j.ijrmhm.2023.106121</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Multigram preparation of tungsten microfibers via needle-less electrospinning of phosphotungstic acid

  • Original language description

    Metallic tungsten microfibers were prepared in a multigram yield by electrospinning from the aqueous phosphotungstic acid/polyvinyl alcohol (PVA) solution in three steps. Green composite microfibers of H3PW12O40 /PVA were easily electrospun from precursor solutions on a Nanospider instrument with a cylindrical rotating electrode. Subsequent oxidation of the organic PVA matrix and decomposition of phosphotungstic acid in the air at 600°C provided ceramic WO3/P2O5 fibers. Finally, prepared oxide fibers were reduced in a forming gas atmosphere at temperatures up to 1000°C. During the reduction, all phosphorus was removed, and pure metallic tungsten microfibers were produced.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10400 - Chemical sciences

Result continuities

  • Project

  • Continuities

    S - Specificky vyzkum na vysokych skolach<br>I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2023

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    International Journal of Refractory Metals and Hard Materials

  • ISSN

    0263-4368

  • e-ISSN

    0263-4368

  • Volume of the periodical

    112

  • Issue of the periodical within the volume

    April

  • Country of publishing house

    GB - UNITED KINGDOM

  • Number of pages

    9

  • Pages from-to

    1-9

  • UT code for WoS article

    000926868100001

  • EID of the result in the Scopus database

    2-s2.0-85146829105