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An experiment and theoretical study of the Cp2VO2CO: use (CO32-)-C-13 for structure investigation of d(1)-metallocene complexes

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216275%3A25310%2F04%3A00001635" target="_blank" >RIV/00216275:25310/04:00001635 - isvavai.cz</a>

  • Result on the web

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    An experiment and theoretical study of the Cp2VO2CO: use (CO32-)-C-13 for structure investigation of d(1)-metallocene complexes

  • Original language description

    EPR study has shown that the anticancer agent vanadocene dichloride (Cp2VCl2) interacts with carbonate contained in physiological solutions. Chelate complex Cp2VO2CO (A(iso)(V-51) = 175.1 MHz, g(iso) = 1.9861) is the only paramagnetic species formed inthe range about the physiological pH (5.5-11.0). The superhyperfine coupling (a(iso)(C-13) = 24.1 MHz) was evidenced at measurements using C-13 labelled carbonate. The structure of carbonate complex was validated by comparison of observed and theoretical calculated HFC tensors (at the density functional level of theory).

  • Czech name

    Experimentální a teoretické studium Cp2VO2CO: použití (CO32-)-C-13 zkoumání struktury d(1)-metalocenových komplexů

  • Czech description

    Experimentální a teoretické studium Cp2VO2CO: použití (CO32-)-C-13 zkoumání struktury d(1)-metalocenových komplexů

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CA - Inorganic chemistry

  • OECD FORD branch

Result continuities

  • Project

  • Continuities

    Z - Vyzkumny zamer (s odkazem do CEZ)

Others

  • Publication year

    2004

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Magnetic Resonance in Chemistry

  • ISSN

    0749-1581

  • e-ISSN

  • Volume of the periodical

    42

  • Issue of the periodical within the volume

    10

  • Country of publishing house

    GB - UNITED KINGDOM

  • Number of pages

    5

  • Pages from-to

    870-874

  • UT code for WoS article

  • EID of the result in the Scopus database