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Crystallography of 2,2',4,4',6,6'-hexanitro-1,1'-biphenyl and its relation to initiation reactivity

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216275%3A25310%2F07%3A00006323" target="_blank" >RIV/00216275:25310/07:00006323 - isvavai.cz</a>

  • Alternative codes found

    RIV/00216275:25310/08:00007945

  • Result on the web

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    Crystallography of 2,2',4,4',6,6'-hexanitro-1,1'-biphenyl and its relation to initiation reactivity

  • Original language description

    X-Ray crystallographic study of 2,2´,4,4´,6,6´-hexanitro-1,1´-biphenyl (HNBP, C12H4N6O12, Mr = 424.21) has been carried out. A possibility of intermolecular hydrogen bonds was indicated and atypically short distances between oxygen atoms of nitro groupsin the 2,6-positions of one molecule and nitro groups in the 4-position of adjacent molecules were found. These interactions might be a reason of the primary reaction of nitro group in the position 4(4´), compared to nitro groups in positions 2,6(2´,6´),in the HNBP molecule during its initiation. In this respect, HNBP differs from the other members of polynitro polyphenylene series containing trinitrophenyl building blocks in their molecules.

  • Czech name

    Krystalografie 2,2',4,4',6,6'-hexanitro-1,1'-biphenylu a její vztah k jeho iniciační reaktivitě

  • Czech description

    Roentgenografická studie of 2,2´,4,4´,6,6´-hexanitro-1,1´-biphenylu (HNBP, C12H4N6O12, Mr = 424.21) byla realizována. Byla indikována možnost existence intermolekulární vodíkové vazby a atypicky krátké vzdálenosti mezi kyslíkovými atomy nitoskupin v 2,6-polohách jedné molekuly a nitroskupin v poloze 4 přilehlé molekuly. Tyto interakce mohou být příčinou primárních reakcí nitroskupiny v poloze 4(4´),v porovnání s nitroskupinami v polohách 2,6(2´,6´), v molekule HNBP během její iniciace. V tomto smyslu seHNBP liší od jiných členů polynitro polyfenylenů, obsahujících v molekule trinitrofenylové stavební jednotky.

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CA - Inorganic chemistry

  • OECD FORD branch

Result continuities

  • Project

  • Continuities

    Z - Vyzkumny zamer (s odkazem do CEZ)

Others

  • Publication year

    2008

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Chemistry of Materials

  • ISSN

    0897-4756

  • e-ISSN

  • Volume of the periodical

    N

  • Issue of the periodical within the volume

    12

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    12

  • Pages from-to

    123-137

  • UT code for WoS article

  • EID of the result in the Scopus database