Voltammetric determination of nitro derivate of synthetic antioxidant 2,6-di-tert-butyl-4-methyl-phenol

Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216275%3A25310%2F16%3A39900406" target="_blank" >RIV/00216275:25310/16:39900406 - isvavai.cz</a>
Result on the web
<a href="http://dx.doi.org/10.1080/00032719.2015.1007376" target="_blank" >http://dx.doi.org/10.1080/00032719.2015.1007376</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1080/00032719.2015.1007376" target="_blank" >10.1080/00032719.2015.1007376</a>

Result language
angličtina
Original language name
Voltammetric determination of nitro derivate of synthetic antioxidant 2,6-di-tert-butyl-4-methyl-phenol
Original language description
A new method is reported for the determination of the nitro derivative of the synthetic antioxidant 2,6-di-tert-butyl-4-methyl-phenol by differential pulse voltammetry with a hanging drop mercury electrode. Standard 2,6-di-tert-butyl-4-methyl-4-nitro-2,5-cyclohexadiene-1-one was synthetizes for voltammetric determination after nitration. A nitration mechanism in acetic anhydride was proposed. The analyte provided a voltammetric signal in a mixture of 0.014 mole per liter potassium chloride and 94% ethanol. The developed method was employed for the determination of 2,6-di-tert-butyl-4-methyl-phenol in oil with satisfactory results, suggesting future application for practical analysis.
Czech name
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Czech description
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Type
J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)
CEP classification
CG - Electrochemistry
OECD FORD branch
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Project
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Continuities
I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Publication year
2016
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

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