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The Molecular and Crystal Structures of 2-Iodokojic Acid: Experimental and Theoretical Determination

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216275%3A25310%2F11%3A39892423" target="_blank" >RIV/00216275:25310/11:39892423 - isvavai.cz</a>

  • Result on the web

    <a href="http://dx.doi.org/10.1007/s10870-011-0051-5" target="_blank" >http://dx.doi.org/10.1007/s10870-011-0051-5</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1007/s10870-011-0051-5" target="_blank" >10.1007/s10870-011-0051-5</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    The Molecular and Crystal Structures of 2-Iodokojic Acid: Experimental and Theoretical Determination

  • Original language description

    The crystal structure of 2-iodokojic acid, (2-jodo-3-hydroxy-6-hydroxymethyl)-4-H-pyran-4-one) (C(6)H(5)IO(4), Mr = 268.00) has been determined by single crystal X-ray diffraction analysis. The compound crystallizes in the orthorhombic crystal system with space group Pc2(1)b and unit cell parameters: a = 4.0830(2), b = 15.3510(5), c = 23.517(1) and Z = 8. The final reliability index is 0.0288 for 2,584 observed reflections. The two molecules of iodokojic acid, slightly differing in their molecular structure, are localized in independent part of unit cell. The crystal packing is stabilized by O-H center dot center dot center dot O hydrogen bonds and I center dot center dot center dot O intermolecular interactions. The molecular structure of iodokojic acid determined experimentally little differs from that obtained by the applied theoretical (Hartree-Fock and four versions of DFT) methods, the differences should not be taken as a measure of the reliability of the theoretical methods. Key

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CA - Inorganic chemistry

  • OECD FORD branch

Result continuities

  • Project

  • Continuities

    Z - Vyzkumny zamer (s odkazem do CEZ)

Others

  • Publication year

    2011

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Journal of Chemical Crystallography

  • ISSN

    1074-1542

  • e-ISSN

  • Volume of the periodical

    41

  • Issue of the periodical within the volume

    8

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    6

  • Pages from-to

    1093-1098

  • UT code for WoS article

    000292838900001

  • EID of the result in the Scopus database