Characterization of 4,6-diazido-N-nitro-1,3,5-triazine-2-amine

Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216275%3A25310%2F12%3A39895763" target="_blank" >RIV/00216275:25310/12:39895763 - isvavai.cz</a>
Alternative codes found
RIV/62690094:18470/12:50000943
Result on the web
<a href="http://onlinelibrary.wiley.com/doi/10.1002/prep.201000166/abstract;jsessionid=C483A8A9ACE2DDDEBCC98F6098DFF6B8.d03t03" target="_blank" >http://onlinelibrary.wiley.com/doi/10.1002/prep.201000166/abstract;jsessionid=C483A8A9ACE2DDDEBCC98F6098DFF6B8.d03t03</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1002/prep.201000166" target="_blank" >10.1002/prep.201000166</a>

Result language
angličtina
Original language name
Characterization of 4,6-diazido-N-nitro-1,3,5-triazine-2-amine
Original language description
4,6-Diazido-N-nitro-1,3,5-triazine-2-amine (DANT) was prepared with a 35?% yield from cyanuric chloride in a three step process. DANT was characterized by IR and NMR spectroscopy (1H, 13C, 15N), single-crystal X-ray diffraction, and DTA. The crystal density of DANT is 1.849 g?cm-3. The cyclization of one azido group and one nitrogen atom of the triazine group giving tetrazole was observed for DANT in a dimethyl sulfoxide solution using NMR spectroscopy. An equilibrium exists between the original DANT molecule and its cyclic form at a ratio of 7?:?3. The sensitivity of DANT to impact is between that for PETN and RDX, sensitivity to friction is between that for lead azide and PETN, and sensitivity to electric discharge is about the same as for PETN. DANT's heat of combustion is 2060 kJ?mol-1.
Czech name
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Czech description
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Type
J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)
CEP classification
CC - Organic chemistry
OECD FORD branch
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Publication year
2012
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

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