Chiral Separation of Benzothiazole Derivatives of Amino Acids using Capillary Zone Electrophoresis
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216275%3A25310%2F17%3A39902304" target="_blank" >RIV/00216275:25310/17:39902304 - isvavai.cz</a>
Result on the web
<a href="http://dx.doi.org/10.1002/jssc.201600689" target="_blank" >http://dx.doi.org/10.1002/jssc.201600689</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1002/jssc.201600689" target="_blank" >10.1002/jssc.201600689</a>
Alternative languages
Result language
angličtina
Original language name
Chiral Separation of Benzothiazole Derivatives of Amino Acids using Capillary Zone Electrophoresis
Original language description
A method for the separation of enantiomers of leucine and phenylalanine benzothiazole derivatives as potential antimicrobial agents was developed using capillary zone electrophoresis with a dual cyclodextrin system. The best resolution of enantiomers was achieved in 100 mmol/L phosphate background electrolyte pH 3.5 with dual cyclodextrin system consisting of 10 mmol/L of beta-cyclodextrin with 10 mmol/L of 2-hydroxypropyl-beta-cyclodextrin for leucine derivative and 10 mmol/L of 2-hydroxypropyl-gamma-cyclodextrin for phenylalanine derivative, respectively. Under the optimal conditions, highest enantioresolution 1.25 was achieved in a non-coated fused silica capillary at 17°C and 24 kV applied voltage.
Czech name
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Czech description
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Classification
Type
J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database
CEP classification
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OECD FORD branch
10406 - Analytical chemistry
Result continuities
Project
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Continuities
I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace
Others
Publication year
2017
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
Journal of Separation Science
ISSN
1615-9306
e-ISSN
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Volume of the periodical
40
Issue of the periodical within the volume
3
Country of publishing house
DE - GERMANY
Number of pages
6
Pages from-to
798-803
UT code for WoS article
000397029500020
EID of the result in the Scopus database
2-s2.0-85007382286