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Silver-Ion Liquid Chromatography–Mass Spectrometry

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216275%3A25310%2F17%3A39910784" target="_blank" >RIV/00216275:25310/17:39910784 - isvavai.cz</a>

  • Result on the web

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    Silver-Ion Liquid Chromatography–Mass Spectrometry

  • Original language description

    Silver-ion high-performance liquid chromatography (Ag-HPLC) coupled to mass spectrometry provides a unique capability to separate molecules according to the number, positions and geometry of double bonds (DB), which can be applied for characterization of the DB arrangement in triacylglycerols, fatty acid methyl esters, and other unsaturated molecules with low to medium polarity. Ag-HPLC is the most reliable technique for the regioisomeric separation of triacylglycerols. Ag-HPLC provides a high orthogonality to reversed-phase HPLC, therefore various configurations of 2D coupling of silver-ion and reversed phase modes give a higher peak capacity for the comprehensive analysis of glycerolipids. The governing factor for the retention order in Ag-HPLC is the total number of DB, which causes the separation of complex mixtures into distinct groups differing in the DB number. The second factor is the DB geometry, where the retention is significantly lower for trans-isomers and finally the smallest effect on the retention is observed for regioisomers.

  • Czech name

  • Czech description

Classification

  • Type

    C - Chapter in a specialist book

  • CEP classification

  • OECD FORD branch

    10406 - Analytical chemistry

Result continuities

  • Project

    <a href="/en/project/LL1302" target="_blank" >LL1302: Mass Spectrometry in Cancer Research: Lipid Biomarkers for Early Diagnostics</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)<br>I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2017

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Book/collection name

    Handbook of Advanced Chromatography /Mass Spectrometry Techniques

  • ISBN

    978-0-12-811732-3

  • Number of pages of the result

    26

  • Pages from-to

    115-140

  • Number of pages of the book

    504

  • Publisher name

    Academic Press (Elsevier)

  • Place of publication

    Cambridge

  • UT code for WoS chapter