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Adsorptive stripping voltammetry of vitamin D3 at glassy carbon electrode

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216275%3A25310%2F18%3A39912550" target="_blank" >RIV/00216275:25310/18:39912550 - isvavai.cz</a>

  • Result on the web

    <a href="https://dk.upce.cz/bitstream/handle/10195/71971/02%20-%20Nallbani%20et%20al.pdf?sequence=1&isAllowed=y" target="_blank" >https://dk.upce.cz/bitstream/handle/10195/71971/02%20-%20Nallbani%20et%20al.pdf?sequence=1&isAllowed=y</a>

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    Adsorptive stripping voltammetry of vitamin D3 at glassy carbon electrode

  • Original language description

    Adsorptive stripping voltammetry (AdSV) of cholecalciferol at the glassy carbon electrode (GCE) was developed and based on existing conventional approaches employing anodic oxidation in pure organic electrolytes or aqueous-organic mixtures. Despite a rather poor reproducibility of the adsorption-driven process (with the RSD of ca. 10 %), significantly higher sensitivity was achieved. As optimum conditions, the respective procedure comprised an accumulation of cholecalciferol from 40% ethanol at 300 min-1 for 8 min followed by electrochemical detection in the Britton-Robinson buffer (pH 4.0) using square-wave voltammetry at a potential step of 5 mV, amplitude of 35 mV, and frequency of 40 Hz.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>ost</sub> - Miscellaneous article in a specialist periodical

  • CEP classification

  • OECD FORD branch

    10406 - Analytical chemistry

Result continuities

  • Project

  • Continuities

    S - Specificky vyzkum na vysokych skolach<br>I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2018

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Scientific Papers of the University of Pardubice, Series A, Faculty of Chemical Technology

  • ISSN

    1211-5541

  • e-ISSN

  • Volume of the periodical

    24

  • Issue of the periodical within the volume

    November

  • Country of publishing house

    CZ - CZECH REPUBLIC

  • Number of pages

    10

  • Pages from-to

    21-30

  • UT code for WoS article

  • EID of the result in the Scopus database