Synthesis of 15N-labelled nitro compounds with a 2,4,6-trinitrophenyl group

Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216275%3A25310%2F20%3A39916495" target="_blank" >RIV/00216275:25310/20:39916495 - isvavai.cz</a>
Result on the web
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DOI - Digital Object Identifier
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Result language
angličtina
Original language name
Synthesis of 15N-labelled nitro compounds with a 2,4,6-trinitrophenyl group
Original language description
The synthesis of 2,4,6-(15N3)-trinitrophenol (picric acid-(15NO2)3), 1-Chloro-2,4,6-(15NO2)3-trinitrobenzene (picrylchloride-(15NO2)3) and various 15N labelled compounds with a 2,4,6-trinitrophenyl (picryl) moiety is described. 15N labelled isotopomers of 2,4,6-trinitroaniline (picramide), N-methyl-N-nitro-2,4,6-trinitroaniline (tetryl) and 3,5-dinitro-N,N´-bis-(2,4,6-trinitrophenyl)pyridine-2,6-diamine (PYX), labelled at different nitrogen atoms were prepared. Potassium (15N)nitrate or sodium (15N)nitrate were used as the source for the (15N)nitro groups. The infrared and Raman spectra of the materials are evaluated, especially the position and shift of (15N)nitro groups. The characteristic infrared and Raman frequencies connected with nitro groups are shifted in the corresponding 15N-labelled materials.
Czech name
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Czech description
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Publication year
2020
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Article name in the collection
Proceedings of the 23nd Seminar on New Trends in Research of Energetic Materials
ISBN
978-80-7560-285-5
ISSN
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e-ISSN
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Number of pages
13
Pages from-to
731-743
Publisher name
Univerzita Pardubice
Place of publication
Pardubice
Event location
Pardubice
Event date
Apr 1, 2020
Type of event by nationality
WRD - Celosvětová akce
UT code for WoS article
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