Synthesis of M1 and M3 alite polymorphs and accuracy of their quantification
The result's identifiers
Result code in IS VaVaI
<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F00216305%3A26110%2F23%3APU146156" target="_blank" >RIV/00216305:26110/23:PU146156 - isvavai.cz</a>
Alternative codes found
RIV/00216224:14310/23:00130260
Result on the web
<a href="https://www.sciencedirect.com/science/article/pii/S0008884622003088" target="_blank" >https://www.sciencedirect.com/science/article/pii/S0008884622003088</a>
DOI - Digital Object Identifier
<a href="http://dx.doi.org/10.1016/j.cemconres.2022.107016" target="_blank" >10.1016/j.cemconres.2022.107016</a>
Alternative languages
Result language
angličtina
Original language name
Synthesis of M1 and M3 alite polymorphs and accuracy of their quantification
Original language description
Although much attention has been paid to the phase analysis of cementitious materials and X-ray diffractometry is nowadays a common tool of quality control, the identification of alite polymorphs is still problematic. A procedure for the laboratory synthesis of monoclinic alite polymorphs in quantities of tens to hundreds grams using mechano-chemical activation and solid-state synthesis was proposed. M1 and M3 alite with a purity of 98 % and 99 % respectively were produced. In order to make the XRD identification in industrial clinkers easier, mixtures of defined ratios of these phases were prepared and generally applicable diffractogram standards were generated. Accuracy of the quantification results via the Rietveld method was verified using the industrial clinker samples with the minor addition of both polymorphs. The profile of the selected reflections is significantly affected by the contents of about 5–10 % of each polymorph.
Czech name
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Czech description
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Classification
Type
J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database
CEP classification
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OECD FORD branch
20501 - Materials engineering
Result continuities
Project
<a href="/en/project/GA20-00676S" target="_blank" >GA20-00676S: Effects of mechano-chemical activation on the process of formation, structure and stability of selected clinker minerals</a><br>
Continuities
P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)
Others
Publication year
2023
Confidentiality
S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů
Data specific for result type
Name of the periodical
Cement and Concrete Research
ISSN
0008-8846
e-ISSN
1873-3948
Volume of the periodical
163
Issue of the periodical within the volume
Leden
Country of publishing house
GB - UNITED KINGDOM
Number of pages
11
Pages from-to
1-11
UT code for WoS article
000891474400002
EID of the result in the Scopus database
2-s2.0-85141271908