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Electron Diffraction Studies on the Modified Z-Phase

Result description

The paper deals with the results of electron diffraction (SAED and CBED) studies on particles of the modified Z-phase in 12CrMoVNbN steels after thermal/creep exposure at 550°C and 600°C. It has been demonstrated that not all diffraction patterns can beindexed using a tetragonal unit cell with dimensions a=0.286nm, c=0.739nm. Some diffraction patterns are consistent with a FCC unit cell with the parameter a=0.404nmn. The FCC unit cell is identical with the FCC subcell in the proposed tetragonal unit cell of the modified Z-phase. In situ transformation of the FCC into the tetragonal unit cell can take place by ordering of metal atom layers along the 001Z direction. The tetragonal Z-phase predominates in diffraction patterns only after long-term thermalexposure.

Keywords

ElectrondiffractionmodifiedZ-phase12CrMoVNbNsteels

The result's identifiers

Alternative languages

  • Result language

    angličtina

  • Original language name

    Electron Diffraction Studies on the Modified Z-Phase

  • Original language description

    The paper deals with the results of electron diffraction (SAED and CBED) studies on particles of the modified Z-phase in 12CrMoVNbN steels after thermal/creep exposure at 550°C and 600°C. It has been demonstrated that not all diffraction patterns can beindexed using a tetragonal unit cell with dimensions a=0.286nm, c=0.739nm. Some diffraction patterns are consistent with a FCC unit cell with the parameter a=0.404nmn. The FCC unit cell is identical with the FCC subcell in the proposed tetragonal unit cell of the modified Z-phase. In situ transformation of the FCC into the tetragonal unit cell can take place by ordering of metal atom layers along the 001Z direction. The tetragonal Z-phase predominates in diffraction patterns only after long-term thermalexposure.

  • Czech name

  • Czech description

Classification

  • Type

    Jx - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    JG - Metallurgy, metal materials

  • OECD FORD branch

Result continuities

Others

  • Publication year

    2007

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Acta Metallurgica Slovaca

  • ISSN

    1335-1532

  • e-ISSN

  • Volume of the periodical

    13

  • Issue of the periodical within the volume

    1

  • Country of publishing house

    SK - SLOVAKIA

  • Number of pages

    7

  • Pages from-to

  • UT code for WoS article

  • EID of the result in the Scopus database

Basic information

Result type

Jx - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

Jx

CEP

JG - Metallurgy, metal materials

Year of implementation

2007