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Ultrathin sectioning of polymeric materials for low-voltage transmission electron microscopy: Relief on ultrathin sections

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F46747885%3A24210%2F03%3A24210127" target="_blank" >RIV/46747885:24210/03:24210127 - isvavai.cz</a>

  • Alternative codes found

    RIV/61389013:_____/03:55033367

  • Result on the web

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    Ultrathin sectioning of polymeric materials for low-voltage transmission electron microscopy: Relief on ultrathin sections

  • Original language description

    Ultrathin sectioning, one of the types of specimen preparations for transmission electron microscopy (TEM), has been considered the most perfect sectioning technique leading to the thinnest sections (50-100 nm). Following a study based on a newly developd low-voltage TEM technique, a relief on the ultrathin sections of polymer blends was observed that was ascribed to substantial differences in mechanical properties of the blend constituents.([1]) In this study, an analogous relief was observed with a blnd, the constituents of which are both hard in cutting. The origin of the surface relief on ultrathin sections of polymer blends was sought using low-voltage scanning TEM and atomic force microscopy. Polycarbonate/styrene-co-acrylonitrile blend was examied as a representative of blends with all components well under T-g at room temperature. A distinct surface relief was observed on both ultrathin sections and remaining cut surfaces of the blend for low-temperature and room-temperature cu

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CD - Macromolecular chemistry

  • OECD FORD branch

Result continuities

  • Project

    <a href="/en/project/IBS4050008" target="_blank" >IBS4050008: Application of the compatibilization of polymer blends for recycling of plastic waste and development of new materials</a><br>

  • Continuities

    Z - Vyzkumny zamer (s odkazem do CEZ)

Others

  • Publication year

    2003

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    J. Macromol. Sci. - Phys.

  • ISSN

    0022-2348

  • e-ISSN

  • Volume of the periodical

    42

  • Issue of the periodical within the volume

    2003

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    8

  • Pages from-to

    1039-1047

  • UT code for WoS article

  • EID of the result in the Scopus database