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Analysis of urinary 8-hydroxy-2´-deoxyguanosine by high-performance liquid chromatography with electrochemical detection

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F49813994%3A_____%2F09%3A%230000016" target="_blank" >RIV/49813994:_____/09:#0000016 - isvavai.cz</a>

  • Result on the web

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    Analysis of urinary 8-hydroxy-2´-deoxyguanosine by high-performance liquid chromatography with electrochemical detection

  • Original language description

    8-hydroxy-2?-deoxyguanosine (8-OH-2?-dG) is one of the predominant forms of radical-induced lesions to DNA, and therefore it has been widely used as a biomarker for oxidative stress. We studied an analytical procedure of determination of urinary 8-OH-2?-dG. A routine assay of free 8-OH-2?-dG in body fluids such as urine is problematic, therefore the purification of this adduct from urine employs solid-phase extraction (SPE) procedure. Various SPE columns from different producers were used as follows: Waters ? Oasis MCX (sorbent silica + benzensulfonic acid), Supelco Discovery C18 Oktadecyl (sorbent silica + C18), UCT Columns ? Clean Screen DAU206 (sorbent silica + C18 + benzenculfonic acid) and Styre Screen DBX (sorbent styrene-divinylbenzene + C18 + benzensulfonic acid), Macherey-Nagel Chromabond HR-X (sorbent styrene-divinylbenzene) and HR-X-C (sorbent styrene-divinylbenzene + benzensulfonic acid), Phenomenex STRATA X-C (sorbent styrene-divinylbenzene + benzensulfonic acid).

  • Czech name

  • Czech description

Classification

  • Type

    D - Article in proceedings

  • CEP classification

  • OECD FORD branch

    10405 - Electrochemistry (dry cells, batteries, fuel cells, corrosion metals, electrolysis)

Result continuities

  • Project

    <a href="/en/project/KAN208130801" target="_blank" >KAN208130801: New design and exploiting nanobiosensors and nanosensors to target medicine (NANOSEMED)</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2009

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Article name in the collection

    International Conference VITAMINS, NUTRITION, DIAGNOSTIC Brno, Czech Republic, August 31 - September 2, 2009 The Abstract Book

  • ISBN

    978-80-7318-809-2

  • ISSN

  • e-ISSN

  • Number of pages

    2

  • Pages from-to

  • Publisher name

    Univerzita Tomáše Bati ve Zlíně

  • Place of publication

    nám. T. G. Masaryka 5555, 760 01 Zlín

  • Event location

    Brno

  • Event date

    Aug 31, 2009

  • Type of event by nationality

    WRD - Celosvětová akce

  • UT code for WoS article