Simultaneous determination of 32 antibiotics in aquaculture products using LC-MS/MS

Result code in IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60076658%3A12520%2F14%3A43886888" target="_blank" >RIV/60076658:12520/14:43886888 - isvavai.cz</a>

Result on the web

<a href="http://link.springer.com/article/10.2478%2Fs11696-013-0428-3" target="_blank" >http://link.springer.com/article/10.2478%2Fs11696-013-0428-3</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.2478/s11696-013-0428-3" target="_blank" >10.2478/s11696-013-0428-3</a>

Result language

angličtina

Original language name

Simultaneous determination of 32 antibiotics in aquaculture products using LC-MS/MS

Original language description

An analytical multiclass, multi-residue method for the determination of antibiotics in aquaculture products was developed and validated. A fast, cheap, and straightforward extraction procedure followed by liquid chromatography-tandem mass spectrometry analysis was proposed. This method covers 32 antibiotics of different classes, which are frequently used in aquaculture. Three different extraction procedures were compared, and the extraction with acetonitrile (0.1 vol. % formic acid) showed the best results. The selected extraction procedure was validated at four different fortification levels (10 mu g kg(-1), 25 mu g kg(-1), 50 mu g kg(-1), and 100 mu g kg(-1)). Recoveries of the tested antibiotics ranged from 70 % to 120 %, with the relative standarddeviation (RSD) of triplicates lower than 20 %. The limits of quantification (LOQ) ranged from 0.062 mu g kg(-1) to 4.6 mu g kg(-1), allowing for the analysis of trace levels of these antibiotics in aquaculture products. The method was ap

Czech name

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Czech description

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Type

J_x - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

CEP classification

DJ - Pollution and water control

OECD FORD branch

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Project

Result was created during the realization of more than one project. More information in the Projects tab.

Continuities

P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)<br>S - Specificky vyzkum na vysokych skolach

Publication year

2014

Confidentiality

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Name of the periodical

Chemical Papers

ISSN

0366-6352

e-ISSN

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Volume of the periodical

68

Issue of the periodical within the volume

1

Country of publishing house

PL - POLAND

Number of pages

8

Pages from-to

29-36

UT code for WoS article

000324491200004

EID of the result in the Scopus database

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