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Thiosugars ? Derivatization agents for the chiral resolution of homoleucines

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60077344%3A_____%2F08%3A00098885" target="_blank" >RIV/60077344:_____/08:00098885 - isvavai.cz</a>

  • Result on the web

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    Thiosugars ? Derivatization agents for the chiral resolution of homoleucines

  • Original language description

    o-Phthaldialdehyde in combination with the series of 6 thiosugars were used for the pre-column chiral derivatization of selected primary amino acids. The diastereomers were resolved on conventional reversed-phase column and with fluorescence detection. Asurprisingly effective resolution of 1-isoindolyl(1-thioglycosides) derived from 1-thio-?-L-fucose was observed.

  • Czech name

    Thiocukry ? Derivatizační činidla pro chirální separaci homoleucinů

  • Czech description

    Pro předkolonovou chirální derivatizaci vybraných primárních aminokyselin byl použit o-ftaldialdehyd v kombinaci se sérií šesti thiocukrů. Vzniklé diastereoisomery byly separovány na konvenční koloně s reverzní fází s využitím fluorescenčního detektoru.Bylo pozorováno překvapivě účinné rozlišení 1-isoindolyl(1-thioglycosidů) odvozených od 1-thio-?-L-fucosy.

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CB - Analytical chemistry, separation

  • OECD FORD branch

Result continuities

  • Project

    <a href="/en/project/GA303%2F06%2F1674" target="_blank" >GA303/06/1674: MULTICOMPLEX DIAGNOSTICS OF B-VITAMIN BIOMARKERS AND NUTRITIONAL STATUS IN PLASMA MICROSAMPLES USING A SIMPLE SAMPLE PRETREATMENT</a><br>

  • Continuities

    Z - Vyzkumny zamer (s odkazem do CEZ)

Others

  • Publication year

    2008

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Journal of Separation Science

  • ISSN

    1615-9306

  • e-ISSN

  • Volume of the periodical

    31

  • Issue of the periodical within the volume

    1

  • Country of publishing house

    DE - GERMANY

  • Number of pages

    4

  • Pages from-to

    133-136

  • UT code for WoS article

  • EID of the result in the Scopus database