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Rapid and senzitive method for citrinin determination using high-performance liquid chromatography with fluorescence detektion

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60162694%3AG44__%2F10%3A00002335" target="_blank" >RIV/60162694:G44__/10:00002335 - isvavai.cz</a>

  • Alternative codes found

    RIV/44555601:13440/10:00005544

  • Result on the web

  • DOI - Digital Object Identifier

Alternative languages

  • Result language

    angličtina

  • Original language name

    Rapid and senzitive method for citrinin determination using high-performance liquid chromatography with fluorescence detektion

  • Original language description

    Citrinin is a toxic product of secondary metabolism of fungi, such as certain Aspergillus, and Monascus species that are usually contaminating cereals. A new sensitive chromatographic method with fluorescence detection was developed, validated, and for citrinin determination. The method is based on reversed-phase separation at 2.5, where citrinin exhibits the highest fluorescence quantum yield. In this setup, no step is needed. The method shows linearity in the range between 0.2 mu g/mL 0.1 mg/mL. The detection limit reached is 90 ng/mL (3.6 x 10(-7) M). Validated method successfully applied on analysis of spiked and real cereal samples.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>x</sub> - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    FP - Other medical fields

  • OECD FORD branch

Result continuities

  • Project

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2010

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Analytical Letters

  • ISSN

    0003-2719

  • e-ISSN

  • Volume of the periodical

    43

  • Issue of the periodical within the volume

    5

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    7

  • Pages from-to

  • UT code for WoS article

    000274995000005

  • EID of the result in the Scopus database