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Novel method for determination of heterocyclic compounds and their impact in brewing technology

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60193697%3A_____%2F21%3AN0000014" target="_blank" >RIV/60193697:_____/21:N0000014 - isvavai.cz</a>

  • Result on the web

    <a href="https://www.kvasnyprumysl.eu/index.php/kp/article/view/242" target="_blank" >https://www.kvasnyprumysl.eu/index.php/kp/article/view/242</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.18832/kp2021.67.417" target="_blank" >10.18832/kp2021.67.417</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Novel method for determination of heterocyclic compounds and their impact in brewing technology

  • Original language description

    A new simultaneous method for determination of 16 heterocyclic compounds using SPE sample preparation and GC-MS determination was developed regarding increasing interest of the role of sensory active compounds in beer. LiChrolut® EN SPE columns proved to be optimal for both, a mixture of analytes with a different polarity and such complicated matrix as beer. Recoveries of individual analytes are about 100% except for three compounds (2-methylpyridine about 30%, maltol and furaneol about 50%); repeatability, uncertainty and LOQ are satisfactory for the method application. The method was used for monitoring of heterocyclic compounds formation during roasting, mashing, hop boiling and fermentation. To summarize, during roasting of malt, the concentration of oxygen heterocycle compounds (OHC) increases more rapidly in comparison with nitrogen heterocycles compounds (NHC) till a critical point where OHC starts to decrease and NHC starts to be formed sharper (with the exception of 2-acetylpyrrole which is similar to OHC). Finally, the total concentration of NHC during fermentation rapidly decreases whilst the OHC concentration is influenced by many factors, e.g., fermentation conditions and yeast strain.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    21101 - Food and beverages

Result continuities

  • Project

  • Continuities

    I - Institucionalni podpora na dlouhodoby koncepcni rozvoj vyzkumne organizace

Others

  • Publication year

    2021

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    KVASNÝ PRŮMYSL

  • ISSN

    2570-8619

  • e-ISSN

    2570-8619

  • Volume of the periodical

    67

  • Issue of the periodical within the volume

    2

  • Country of publishing house

    CZ - CZECH REPUBLIC

  • Number of pages

    11

  • Pages from-to

    417-427

  • UT code for WoS article

    000662244400001

  • EID of the result in the Scopus database