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Redox-switchable alpha-diimine palladium catalysts for control of polyethylene topology

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60461373%3A22310%2F19%3A43918218" target="_blank" >RIV/60461373:22310/19:43918218 - isvavai.cz</a>

  • Alternative codes found

    RIV/00216208:11310/19:10398748

  • Result on the web

    <a href="https://www.sciencedirect.com/science/article/pii/S0032386119306032" target="_blank" >https://www.sciencedirect.com/science/article/pii/S0032386119306032</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1016/j.polymer.2019.121619" target="_blank" >10.1016/j.polymer.2019.121619</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Redox-switchable alpha-diimine palladium catalysts for control of polyethylene topology

  • Original language description

    A series of palladium complexes bearing ferrocene substituted alpha-diimine ligands was synthesized and investigated for ethene polymerization at different conditions to modulate the extent of &quot;chain-walking&quot; mechanism and regulate branching and topology of resulting polyethylenes. All ferrocene substituted complexes catalyzed living/controlled ethene polymerization. The ability of ferrocene substituted palladium complexes to provide polyethylenes with dendritic topology was proved by measuring their Mark-Houwink plots. In-situ chemical oxidation of ferrocene moieties via silver triflate was used to affect the catalyst electronic structure and support the &quot;chain-walking&quot; mechanism. Oxidation of palladium catalyst led to its destabilization while the catalytic activity of newly formed sites was substantially increased. It was demonstrated that catalyst oxidation is a powerful tool to regulate the topology of resulting polyethylenes.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10403 - Physical chemistry

Result continuities

  • Project

    Result was created during the realization of more than one project. More information in the Projects tab.

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2019

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Polymer

  • ISSN

    0032-3861

  • e-ISSN

  • Volume of the periodical

    179

  • Issue of the periodical within the volume

    28.6.2019

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    12

  • Pages from-to

  • UT code for WoS article

    000487254600041

  • EID of the result in the Scopus database