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Azide Decomposition as a Pathway to Intramolecularly Upper-Rim-Bridged Calix[4]arenes

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60461373%3A22310%2F22%3A43924475" target="_blank" >RIV/60461373:22310/22:43924475 - isvavai.cz</a>

  • Result on the web

    <a href="https://www.thieme-connect.de/products/ejournals/abstract/10.1055/a-1668-9694" target="_blank" >https://www.thieme-connect.de/products/ejournals/abstract/10.1055/a-1668-9694</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1055/a-1668-9694" target="_blank" >10.1055/a-1668-9694</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Azide Decomposition as a Pathway to Intramolecularly Upper-Rim-Bridged Calix[4]arenes

  • Original language description

    Proximally single-atom-bridged calix[4]arenes possess a rigidified cavity and, thus, unusual complexation properties. Here, we report on the synthesis of the first such heteroatom-bridged compound: amine-bridged calix[4]arene. This compound, prepared by thermal decomposition of 4-azidocalix[4]arene, was obtained alongside very interesting rearranged, inherently chiral 10H-azepino[1,2-a]indole derivatives. NMR titration confirmed the suitability of the amine cavity for the complexation of methylammonium cations; moreover, the -NH- bridge function enables its further derivatization. © 2021. Thieme. All rights reserved.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10401 - Organic chemistry

Result continuities

  • Project

    <a href="/en/project/GA20-07833S" target="_blank" >GA20-07833S: New nanomaterials for anion separation</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Others

  • Publication year

    2022

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Synthesis

  • ISSN

    0039-7881

  • e-ISSN

    1437-210X

  • Volume of the periodical

    54

  • Issue of the periodical within the volume

    5

  • Country of publishing house

    DE - GERMANY

  • Number of pages

    8

  • Pages from-to

    1301-1308

  • UT code for WoS article

    000726981200002

  • EID of the result in the Scopus database

    2-s2.0-85121121148