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Determination of Diaryliodonium Species by Reverse Iodometric Titration with Ascorbic Acid

The result's identifiers

  • Result code in IS VaVaI

    <a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60461373%3A22310%2F23%3A43924275" target="_blank" >RIV/60461373:22310/23:43924275 - isvavai.cz</a>

  • Result on the web

    <a href="https://analyticalsciencejournals.onlinelibrary.wiley.com/doi/10.1002/elan.202200376" target="_blank" >https://analyticalsciencejournals.onlinelibrary.wiley.com/doi/10.1002/elan.202200376</a>

  • DOI - Digital Object Identifier

    <a href="http://dx.doi.org/10.1002/elan.202200376" target="_blank" >10.1002/elan.202200376</a>

Alternative languages

  • Result language

    angličtina

  • Original language name

    Determination of Diaryliodonium Species by Reverse Iodometric Titration with Ascorbic Acid

  • Original language description

    Diaryliodonium salts are used in organic chemistry, materials science and pharmaceutical chemistry. For the quantitative analysis of diaryliodonium salts, only instrumentally demanding techniques requiring highly skilled operators are available. Surprisingly, no titration method taking advantage of the oxidising ability of diaryliodonium is available in the literature. In the present work, a titration method for the determination of diaryliodonium salts is presented. It is based on the reaction of diaryliodonium species with ascorbic acid, whose excess is subsequently determined by means of iodometric potentiometric titration. Application of the protocol to various diaryliodonium salts revealed the scope and limitations of the method. © 2023 Wiley-VCH GmbH.

  • Czech name

  • Czech description

Classification

  • Type

    J<sub>imp</sub> - Article in a specialist periodical, which is included in the Web of Science database

  • CEP classification

  • OECD FORD branch

    10406 - Analytical chemistry

Result continuities

  • Project

    <a href="/en/project/EF16_025%2F0007445" target="_blank" >EF16_025/0007445: Organic redox couple based batteries for energetics of traditional and renewable resources.</a><br>

  • Continuities

    P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)<br>O - Projekt operacniho programu

Others

  • Publication year

    2023

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Electroanalysis

  • ISSN

    1040-0397

  • e-ISSN

    1521-4109

  • Volume of the periodical

    35

  • Issue of the periodical within the volume

    5

  • Country of publishing house

    DE - GERMANY

  • Number of pages

    9

  • Pages from-to

    nestránkováno

  • UT code for WoS article

    000891971700001

  • EID of the result in the Scopus database

    2-s2.0-85142922087