Analysis of anabolic androgenic steroids by direct analysis in real time ionization with time-of-flight mass spectrometry

Result code in IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60461373%3A22330%2F15%3A43899512" target="_blank" >RIV/60461373:22330/15:43899512 - isvavai.cz</a>

Result on the web

<a href="http://www.sciencedirect.com/science/article/pii/S1387380615002730" target="_blank" >http://www.sciencedirect.com/science/article/pii/S1387380615002730</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.1016/j.ijms.2015.08.022" target="_blank" >10.1016/j.ijms.2015.08.022</a>

Result language

angličtina

Original language name

Analysis of anabolic androgenic steroids by direct analysis in real time ionization with time-of-flight mass spectrometry

Original language description

We verified applicability of direct analysis in real time ionization coupled with a time-of-flight mass spectrometer (DART-MS) for detection of anabolic androgenic steroids in supplements and pharmaceuticals. DART-MS was optimized for the analysis of eleven frequently misused anabolic androgenic steroids and their derivatives. Real supplement tablets and injectable oil solutions were used to verify applicability of the method. It was found that anabolic androgenic steroids can be analyzed directly without any sample pre-treatment, which reduces the sample preparation time and hence the overall analysis time. The resulting DART-MS method is suitable for rapid routine qualitative screening of anabolic androgenic steroids in simple sample matrices. It has a great potential in the field of adulterated and counterfeited anabolic steroid pharmaceuticals and supplements.

Czech name

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Czech description

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Type

J_x - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

CEP classification

CB - Analytical chemistry, separation

OECD FORD branch

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Project

<a href="/en/project/VG20112015045" target="_blank" >VG20112015045: Rapid immunochemical tests for the detection of steroidal anabolics</a><br>

Continuities

P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Publication year

2015

Confidentiality

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Name of the periodical

International Journal of Mass Spectrometry

ISSN

1387-3806

e-ISSN

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Volume of the periodical

392

Issue of the periodical within the volume

DEC 3 2015

Country of publishing house

NL - THE KINGDOM OF THE NETHERLANDS

Number of pages

6

Pages from-to

28-33

UT code for WoS article

000366441700005

EID of the result in the Scopus database

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