Monitoring survey of patulin in a variety of fruit-based products using a sensitive UHPLC-MS/MS analytical procedure

Result code in IS VaVaI

<a href="https://www.isvavai.cz/riv?ss=detail&h=RIV%2F60461373%3A22330%2F15%3A43900589" target="_blank" >RIV/60461373:22330/15:43900589 - isvavai.cz</a>

Result on the web

<a href="http://www.sciencedirect.com/science/article/pii/S095671351400454X" target="_blank" >http://www.sciencedirect.com/science/article/pii/S095671351400454X</a>

DOI - Digital Object Identifier

<a href="http://dx.doi.org/10.1016/j.foodcont.2014.07.064" target="_blank" >10.1016/j.foodcont.2014.07.064</a>

Result language

angličtina

Original language name

Monitoring survey of patulin in a variety of fruit-based products using a sensitive UHPLC-MS/MS analytical procedure

Original language description

The mycotoxin patulin is known to be the predominant natural contaminant of apples, apple-based products and a variety of other fruits. Because of its high incidence and harmful health effects, patulin is included with mycotoxins, which are strictly monitored. In this study, a sensitive and reliable ultra-high performance liquid chromatography-tandem mass spectrometry (UHPLC-MS/MS) method was developed and validated for determination of patulin in a variety of fruit matrices. A combination of the QuEChERS (Quick, Easy, Cheap, Effective, Rugged and Safe) procedure along with a solid phase extraction (SPE) clean-up strategy enabled an effective removal of sample matrix and pre-concentration of patulin. This resulted in low limits of quantification ranging from 1 to 2.5 mu g/kg, depending on fruit type. In our study, quantification of patulin was based on a stable isotope dilution assay (SIDA) using C-13(7)-patulin as the internal standard. Data showed that the procedure described, in com

Czech name

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Czech description

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Type

J_x - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

CEP classification

GM - Food industry

OECD FORD branch

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Project

Result was created during the realization of more than one project. More information in the Projects tab.

Continuities

P - Projekt vyzkumu a vyvoje financovany z verejnych zdroju (s odkazem do CEP)

Publication year

2015

Confidentiality

S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Name of the periodical

Food control

ISSN

0956-7135

e-ISSN

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Volume of the periodical

47

Issue of the periodical within the volume

JAN 2015

Country of publishing house

BE - BELGIUM

Number of pages

8

Pages from-to

577-584

UT code for WoS article

000343612700081

EID of the result in the Scopus database

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