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An in situ UV-vis and FTIR spectroscopy study of the effect of H2 and CO during the selective catalytic reduction of nitrogen oxides over a silver alumina catalyst

Result description

he effect of hydrogen and carbon monoxide on the selective catalytic reduction of NOx with decane over a 2 wt% Ag/Al2O3 catalyst was investigated. Hydrogen promoted NOx conversion during the SCR reaction, in contrast to carbon monoxide, which had a slightly detrimental effect on catalyst activity, However, in situ UV-vis spectroscopy showed that both carbon monoxide and hydrogen promoted the formation of Ag clusters during the reaction. This, coupled with previous EXAFS experiments and UV-vis data on the rate of change of cluster formation, demonstrate that the enhanced activity from the addition of hydrogen to the NOx-SCR mix cannot be attributed exclusively to the formation of Ag clusters. It is proposed that hydrogen itself participates directly inthe reaction mechanism.

Keywords

SCR-NOxAg/aluminaAg clustersH2 effect in SCR-NOx

The result's identifiers

Alternative languages

  • Result language

    angličtina

  • Original language name

    An in situ UV-vis and FTIR spectroscopy study of the effect of H2 and CO during the selective catalytic reduction of nitrogen oxides over a silver alumina catalyst

  • Original language description

    he effect of hydrogen and carbon monoxide on the selective catalytic reduction of NOx with decane over a 2 wt% Ag/Al2O3 catalyst was investigated. Hydrogen promoted NOx conversion during the SCR reaction, in contrast to carbon monoxide, which had a slightly detrimental effect on catalyst activity, However, in situ UV-vis spectroscopy showed that both carbon monoxide and hydrogen promoted the formation of Ag clusters during the reaction. This, coupled with previous EXAFS experiments and UV-vis data on the rate of change of cluster formation, demonstrate that the enhanced activity from the addition of hydrogen to the NOx-SCR mix cannot be attributed exclusively to the formation of Ag clusters. It is proposed that hydrogen itself participates directly inthe reaction mechanism.

  • Czech name

    In-situ UV-Vis a FTIR spektroskopická studie efektu H2 a CO na selektivní katalytickou redukci oxidů dusíku na katalyzátoru Ag/alumina

  • Czech description

    Byl studován efekt vodíku a oxidu uhelnatého na selektivní katalytickou redukci oxidů dusíku dekanem na katalyzátoru 2 hm.% Ag/Al2O3. Vodík zvyšuje konverzi během selektivní katalytické redukce, na rozdíl od oxidu uhelnatého, který má mírně nepříznivý efekt na katalytickou aktivitu. Nicméně, in-situ UV-Vis spektra ukázala, že jak vodík tak oxid uhelnatý podporují tvorbu nabitých klastrů. Toto, společně s předcházejícími EXAFS experimenty a UV-Vis daty rychlosti formování klastrů ukazuje, že zvýšení aktivity přidáním vodíku do reakční směsi nemůže být exklusivně připsáno vzniku klastrů stříbra. Vodík samotný participuje v reakčním mechanizmu.

Classification

  • Type

    Jx - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

  • CEP classification

    CF - Physical chemistry and theoretical chemistry

  • OECD FORD branch

Result continuities

Others

  • Publication year

    2005

  • Confidentiality

    S - Úplné a pravdivé údaje o projektu nepodléhají ochraně podle zvláštních právních předpisů

Data specific for result type

  • Name of the periodical

    Journal of Catalysis

  • ISSN

    0021-9517

  • e-ISSN

  • Volume of the periodical

    235

  • Issue of the periodical within the volume

    1

  • Country of publishing house

    US - UNITED STATES

  • Number of pages

    6

  • Pages from-to

    195-200

  • UT code for WoS article

  • EID of the result in the Scopus database

Basic information

Result type

Jx - Unclassified - Peer-reviewed scientific article (Jimp, Jsc and Jost)

Jx

CEP

CF - Physical chemistry and theoretical chemistry

Year of implementation

2005